GCMS analysis results for sample AD27768, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27768.D Vial: 11 Acq On : 20 Dec 2001 5:02 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 3-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD ■ R.T.

6.73 2.04 ng/uL 679347 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hi xano l 102 C6H140 000623-37-0 83 Abundance < Scan 206 (6.728 min): 27768.D (-) m/ z 59.10 100.00% 55 59

5000- 73 43 . rA —— —

miz-> r " • i" ’ • i m 39 51 T-p-r 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 +4 Tpm 1T 84 i1 ‘' i r"•i 101 11 ‘11' I v 6.40 m/ Z 6.60 55.10 6.80 7.00 83.17% Abundance #63527: 3-Hexanol — 59 55

73 r i i । ।4।-। | । । r । | 5000- 31 6.40 6.60 6.80 7.00 m/z 73.05 44.23% 27 45 TT TTTTTT — T 1................. TT 84 • I ' 1 " pTTTp-rrrpTTTT r " ■ i ■ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762: 3-Hexanol 59 55 yuu TTInnnnnn/n TT|-rrr i I 31 6.40 6.60 6.80 7.00 5000 27 43 73 m/z 43.10 30.79%

TTTTTTT’TT 102 Ji p-rr TTTTTTTTTTT TT M i " " i" " i ■ I " " I । ■ ■ ■ ■ । m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529:3-Hexanol TII—unnrT ■ • | ■ • • ■ | 55 59 6.40 m/ z 6.60 6.80 7.00 41.10 23.30% 31 5000 73

Mai 27

44 mH 4) ImH TT1'1 ' I | ! । । । | 102 1 r । । " > । i TTf n r• i TT m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00

27768.D NP112701.M Thu Dec 20 11:46:39 2001 Page 3

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