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GC/MS analysis results for sample AD23321, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23321 conducted on October 15, 2001.

NYC-WTC_000088237–000088262

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088252
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23321.D Vial: 14 Acq On : 12 Oct 2001 2:50 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Butyl tetradecanoate (myristat Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.64 2.39 ug/1 300053 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butyl t^tradecanoate (myristate) 284 C18H36O21 000000-00-0 72 2 2-Met^1-N-1 - tridecene 196 C14H28 018094-01-4 27 3 Cycloloutane, 1, l-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 4 l-HQk:ene, 2-methyl- 98 C7H14 006094-02-6 27 Abundance/ Scan 2897 (31.639 min): 23321 .D (-) m/z 56770 0 1 00.00% 5

5000 4- 73 129 OCT 285 .............. ......................... 9^ I 157 y 241 T I 340 31.40 31.60 31.80 32.00 rrtrr Wz 57700 53.91% ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 55

5000 229 31.40 31.60 31.80 32.00 m/z 43.05 44.81%

■Tl/Z-> 20 I'' " I' 40 60 T. 129 t I I ''''I' " rI" ' ' I 211

I I ... I . . i-rp-f I . I ■ ri I f 80 100 120 140 160 180 200 220 240 260 280 300 320 340 284 4^ <U3undance #21975: 2-Methyl-N-1-tridecene 55 1 31.40 31.60 31.80 32.00 5000 m/z 41.05 38.47%

27 I 83 I i I 140 168 196 I' '' ' I' ' ' ' I I'' '' I 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #21985: Cyclobutane, 1,1-dimethyl-2-octyl- -CT '-'7" " I. 5 31.40 31.60 31.80 32.00 m/z 55700 31774%

5000

27 I I'''' I' pTVrTTrriYrT+TprTTT-|TTTr^ I ’'' ' I ' '' ' I I'''' I '' •' I t-p- ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23321.D NP091101.M Mon Oct 15 10:22:30 2001 Page 8

NYC-WTC_000088252

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NYC-WTC_000088252Source: NYC Law Department, mirrored locally

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