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GC/MS analysis results for sample AD23079, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087794–000087816

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0301\23079.D Vial: 6 Acq On 3 Oct 2001 5:32 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★ Peak Number 12 Heneicosane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

35.52 0.95 ug/1 114387 Perylene-dl2 37.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Hexatriacontane 507 C36H74 000630-06-8 91 3 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91 4 Nonacosane 408 C29H60 000630-03-5 91. (Abundance Scan 3320 (35.522 min); 23079.D (-) m/z 57.00 100.00% 57 43 71 85 5000

1 ( 1 ^113 T J I 1 1.11 J 1^^1411W169183 208 239253 281 35.20 35.40 35.60 35.80 I I TI I T I I i l l I I j I I T I I I I I I p I 11 I b r I I I I I I I I I I t "| I I I I j r I r' I I I I I I | I I'''' I'''' I m/z 43.05 69.20% 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 1 i i 71 95 5000 35.20 35.40 35.60 35.80 99 m/z 71. on 67.62% J J J TT’1”?’ I'' ’' I 268 I'''' I'''' I' 296 I'''' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Atbundance #74636; Hexatriaconlane 43 57 . . 1*. , I . f . 7', r I . . p 71 35.20 35.40 35.60 35.80 I 5000 ' 85 m/z 85.0,5 51.16%

3 [ 113127141155169183197211 p-rTTp-rTT-p-rTTyTTTTjTTTT-TpTr-TTYTTT-TyTTn^ I I .1 . I . . < . jT^i . q > . > . I . . . . } m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #51002; Heneicosane, ll-(l-ethylpropyl)- 43 57 35.20 35.40 35.60 35.80 m/z 54.95 21.85% 71 5000 85

113127141183197211225 295 338 \Aaaa 'I''''I''''I '''' I' '' ' I hi/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 35.20 35.40 35.60 35.80

23079.D NP091101.M Tue Oct 09 09:58:22 2001 Page 12

NYC-WTC_000087812

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NYC-WTC_000087812Source: NYC Law Department, mirrored locally

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