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GC/MS analysis results for sample AD23345, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23345 conducted on October 16, 2001.

NYC-WTC_000088556–000088584

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088579
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0901\23345.D Vial: 17 Acq On : 10 Oct 2001 4:57 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 17 Tetratetracontane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 36.36 3.89 ug/1 293856 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetratetracontane 619 C44H90 007098-22-8 91 2 Tetracosane 338 C24H50 000646-31-1 91 3 Heneicosane 296 C21H44 000629-94-7' 91 4 Eicosane, 7-hexyl-__________________ 366 C26H54 055333-99-8 91 Abundance Scan 3411 (36.357 min): 23345.D (-) m/z 57700 100.00% 57

85

Ji 5000

36.00 36.20 36.40 36.60 .^3211 267 ....... ......... m/z 70795 73761% Ti/z-> Abundance 50

57 100 150 200 250 300 350 400 #61068: Tetratetracontane 450 500 550 600 ft 5000 85 ‘ 36.00 36.20 36.40 36.60 m/z 43.00 64.76%

Ti/z-> 50 100 !* 150 200 .......... ................. 250 300 350 400 450 500 550 600 ft Abundance #73543: Tetracosane 57 A 36.00 36.20 36,40 36.60 5000 85 m/ Z ■ 85.05 49.28%

ft nn/z-> Abundance 50

57 100 150 200 250 300 350 400 #42201: Heneicosane 450 500 550 600 R 36.00 36.20 36.40 36.60 m/z 55.00 26.83% 85 5000

.... ........................... 71/Z~> 50 100 150 200 250 300 350 400 450 500 550 600 36.00 36.20 36.40 36.60

23345.D NP091101.M Thu Oct 11 13:10:47 2001 Page 17

NYC-WTC_000088579

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