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GCMS results log, sample AD26987, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26987 completed on December 11, 2001.

NYC-WTC_000032427–000032447

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 6 01\26987.D Vial: 26 Acq On 7 Dec 2001 8:54 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 12 Hexane, 2,2,3,3-tetramethyl- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

36.40 0.51 ng/uL- 131217 Perylene-dl2 37.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexane, 2 ,2, 3,3 -tetramethyl - 142 C10H22 013475-81-5 47 2 Heptadecane 240 C17H36 000629-78-7 42 3 Heptane,/2,4,6-trimethyl- 142 C10H22 002613-61-8 38 4 Ether, hexyl pentyl 172 C11H240 032357-83-8 38 Abundance Scan 3442 (36.403 min): 26987.D (-) m/z 57. ,0 100.00% i 57 43 71 5000- 85

97 IAAAA—4 lilt । ■ ■ ■ ■ । ■ AL—................. ..... — m/z-> 20 40 60 80 ___ 100 120 140 160 180 200 220 240 Abundance #8106: Hexane, 2,2,3,3-tetramethyl- 43 57

5000 85 ArMAM 36.00 36.20 36.40 36.60 36.80 |

X 71 99 m/ z 71. Q05 <62.28% 'i ■ II 1 ■ ■ i i miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #71191: Heptadecane 57 43 A ■ • ■ ' i ■ ■ NA.. 1,1 ’ I • ' 71 36.00 36.20 36.40 36.60 36.80 5000 m/z 85.05 49.61% 85

l 99 113 127 141 240 i i ■ ■ ■ ■ i ■ ' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #8089: Heptane, 2,4,6-trimethyl- 43 85 36.00 36.20 36.40 36.60 36.80 57 m/z 55.L0 32.13% 5000

! 27 71 — 99 — 1......... 127 142............................................ ' — m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 36.00 36.20 3640 36.60 36.80

26987.D NP112701.M Tue Dec 11 14:53:05 2001 Page 12

NYC-WTC_000032446

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