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GCMS results log, sample AD26985, Dec 11 2001

Machine-extracted title · confidence 95%

Laboratory report for GCMS analysis of sample AD26985 completed on December 11, 2001, showing surrogate recovery.

NYC-WTC_000032400–000032426

Folder label: “GCMS X 11/8/01 A 12/7/01

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Scanned page image, NYC-WTC_000032425
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26986.D Vial: 32 Acq On 7 Dec 2001 3:19 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 17 Heptadecane Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

35.55 0.62 ng/uL 188930 Perylene-dl2 37.28

Hit# of 5/ Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 42 2 Hexane/ 2,2,3,3-tetramethyl- 142 C10H22 013475-81-5 38 3 Ether/ heptyl hexyl 200 C13H280 007289-40-9 38 4 Hex. ecane 226 C16H34 000544-76-3 36 Abundance Scan 3349 (35.549 min): 26986.D (-) m/z 57.10 100.00% 57

43 71 5000- 85 A4--A44------I----TYA 99 ... 35.20 35.40 35.60 35.80 • — il 111 I IIr m/z 43. 10 61.22% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #71191: Heptadecane 57 43 71 am AA 44 5000 85 35.20 35.40 35.60 35.80 m/ Z 71.05 59.97% f ' ‘ 1 ' i 1 11 ___ i ■ ■ i! , 99 113 127 141 ............ 240 m/z->20 40 60 80 100 120 140 160 180 200 220 240 ‘Abundance #8106: Hexane, 2.2.3,3-tetramethyl- 43 57 • ■ i ■ ■ TTT 35.20 35.40 35.60 35.80 I 5000- 85 m/z 85.15 40.14% 71 99 . i 1 ‘ 1 ■ । ■ m/z-> 20 40 60____ 80 100 120 140 160___ 180__ 200 220 240 Abundance #23013: Ether, heptyl hexyl 1 ' i 1 1 ■ ■ i ■ ■ 1 1 i ■ ■ y 1 I ' 1 1 1 1 1 57 35.20 35.40 35.60 35.80 43 m/ z 41.10 23.86% 5000- 85

m/z--> 20 27 I । I I ' ■ ■ ■ i ' ' 40 70 . , 1 , 1 , 97L ’I' * 1 ' 1 1 60 80 100 115 120 ................................................... 140 160 180 200 220 240 1 1 i ' . Mm 35.20 35.40 35.60 35.80

26986.D NP112701.M Tue Dec 11 14:51:52 2001 Page 17

NYC-WTC_000032425

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NYC-WTC_000032425Source: NYC Law Department, mirrored locally

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