GCMS analysis results for sample AE06452, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1702\6452.D Vial: 10 Acq On : 17 Apr 2002 5:02 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 3-Isopropoxy-l, 1,1,7,7,7-hexam Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

37.31 1.06 ug/1 85416 Perylene-dl2 37.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropo^y-l,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 32 2 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 32 3 3 -Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 22 4 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 22 Abundance Scan 3514 (37.309 min): 6452.D (-) m/z 73.00 100.00% 73 147 5000 221 281 355 I . > I I I . > I I I 429

mlz—> 44 , ■ ■ 1 50 100 1 177 150 200 250 2534 300 350 L327L1 401L 400 450 500 550 37.00 37.20 37.40 37.60 m/z 147.00 64.53% Abundance #60503: 3-lsopropoxy-1,1,1,7,717-hexamethyl-3,5,5-tris(trim 73

5000 1 1 I ' ' 1 * I 147 37.00 37.20 37.40 37.60 m/z 221.05 50.62% 1 ' i T 21.21327 I 1 I I I I 1 I I I I I I I TT 415 1 I I I I J I TI 1T 519 561 I 1I I I I I "1 TI I T T mlz—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 221 A AMAMR r ( T 1 1 । 1 1 1 ' I 73 37.00 37.20 37.40 37.60 5000 m/z 355.05 33.63% 191 117 279

m/z-> 50 1 ' i —4 100 III 150 200 i 250 300 350 400 450 500 550 Abundance #56734:3-Trimethyisilyloxystearic acid, trimethylsilyl est AAAAAAAL 73 37.00 37.20 37.40 37.60 m/z 281.00 28.86% 5000

m/z—> ■ ■ । > * > ■ । 50 100 147

■ i ‘ i 150 189

200 233

... , 4 , I ' ,1 i ■ ■ 250 300 313 339I 1 1 1 ' I 1 ' 1 ■ i ■ 1 ' ■ 387 350 400 429 ’ 1 I 1 1 ' ■ I ' 1 ' 1 1 1 ‘ 450 500 550 ] “WVAA

37.00 37.20 37.40 37.60

6452.D GCMS0412.M Thu Apr 18 09:12:20 2002 Page 3

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