GCMS analysis results, sample AE04947, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR3OO2\4947.D Vial: 14 Acq On : 30 Mar 2002 3:51 am Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyciopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.85 2.05 ug/1 327044 Naphthalene-d8 15.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 Phenethylamin^, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 47 3 N-(Trifluoroa/etyl)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 38 4 Benzoic acid,. 2-[(trimethylsilyl)ox 282 C13H22O3Si2 003789-85-3 32 Abundance 73 Scan 1068 (14.847 min): 4947.D (-) m/ Z 737'0,0....icToTo^

5000 267 355

45 108 133'154 193 223 _____ 14.60 14.80 15.00 15.20 _ 293 323 ............ m/z 2 67.00"" 45780% m/z-> 50 10.0... -150 200 250 300 350 400 450 Abundance #51266: Cyciopentasiloxane, decamethyl- 73

355 267 5000 I ' ' 14.60 14.80 15.00 15.20 m/z 3 557op 43.83% ...... 207 I, 323 'm/z-^L____ ,50. ___ log__ 150 200 250 300 350 400 450 Abundance #7^23: PI'entrhyiaiTune N-rriethyl-.t)e'ta.,3,4-tns(tri:Tiethyls 73 -pT-r \ 14.60 14.80 15.00 15.20 5000 355 m/z 356.05" 17.33% 44 147 JI93^ ni/z-> 50 100 150 200 250 300 350 400 450 Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-lris(trimethyisilyl)no 713 14.60 14.80 15.00 15.20 355 m/z 268.00 " 11.63% 5000

45 I 126147 193 265 376 481 . ..... M. ............. 'm/z-> 50 100 150 200 250 300 350 400 450 14.60 14.80 15.00 15.20

4947.D GCMS0308.M Tue Apr 02 11:10:18 2002 Page 1

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