GCMS analysis page, sample AE05033, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2602\5033.D Vial: 25 Acq On : 27 Mar 2002 9:31 am Operator: Sample : gc/ms scan 3/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyciopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.85 0.95 ug/1 200461 Naphthalene-d8 15.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasilo^ne, decamethyl- 370 C10H3005Si5 000541-02-6 86 2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H32O3Si3 068595-79-9 46 3 Benzoic acidl 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 38 4 Phenethylan/ne, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 Abundance 7|3 Scan 1068 (14.847 min): 5033.D (-) m/'z. .. 737oo’”70o'/OO%i

5000 267 355

45 108 133 154 177193 223 251 , 323339I 14.60 14.80 15.00 15.20 p-rrTjT-TT-rp-TYTp-rTSY’-T-Tm'YTTVrp'VT^^ m/z 267.00’ 44.57% m/z-> 40 60 80100 120140 160 180 200 220 240 260 280 300 320 340 360 'Abundance #51266: Cyciopentasiloxane, decamethyl- 70

355 267 •p-e ‘ I ' ' 5000 14.60 14.80 15.00 15.20 m/z 355.05 42.55% 191207 2?^ I 323 339 m/_z->___ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #40828: dA-Oibydroxybenzyl aicotioi.irisiirimettiyisiiyl)- 73 -p-r 14.60 14.80 15.00 15.20 267 5000 179 m/z 356.05 15.79% 356 45 147 209 237 i 312 341 '''' I'''' I'' ’' I' ''' I ''' 11"' ’ I'"' r m/z-> Abundance 40 60 73 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 #7*3975: Benzoic acid, 2,4-bis[(trimethylsiiyi)oxyj-, trimet n 14.60 14.80 15.00 15.20 m/ z 2 68.00 12.04% I i 5000 355 45 133 149 193 223 340 370 281 I'''' I'' ——— m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15.00 15.20

5033.D GCMS0308.M Fri Mar 29 11:37:43 2002 Page 1

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