GCMS chromatogram data for sample AE04592, April 2002

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Data File : C:\HPCHEM\l\DATA\MAR2602\4592.D Vial: 8 Acq On : 26 Mar 2002 4:38 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

40.59 4.66 ug/1 386122 Perylene-dl2 37.94

Hit# of 5 Tentative ID MW . MolForm CAS# Qual 1 3,6-Dioxa-2,4,5,7-te^asilaoctane, C10H3002Si4 294 004342-25-0 32 2 Trisiloxane, 1,1,1,^5,5-hexamethyl C12H36O4Si5 384 003555-47-3 22 3 l,l,l,5,7,7,7-Hept^ethyl-3,3-bis(t C13H40O5Si6 444 038147-00-1 13 4 3-Isopropoxy-1,1,7,7,7-hexamethyl C18H52O7Si7 576 071579-69-6 10 Abundance........ .......... Scan 3872 (40.595min):4592U(-)............ m/ z 73 147 221 5000 281 355 429 40.20 40.40 40.60 40.80 41.00 117 177 401 , I' ‘' 'I' rrYp- pT7-rpTTTY'-rTTp‘trT^p-rmTyrTT'ry^ P m/z 147.00 70.75% .m/z~> 40 60 80 100120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance Ml682: i6-Dioxa-2,4,5,7-tetrasiiaoctarie, 2,2,44,5,57,7/........ . "147 2: !1

73 5000 40.20 40.40 40.60 40.80 41.00 191 117 279 m/z .’46% I p-TTTp-rJfTT-rTpTTTYr^-rrjT-rTTiTT^^ I I I 'm/z->___ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance ’'••7^103;'rnsHoxane. i l.i,5 S.S-re.iaiT^eliyi-S.S-bisKliP'iet 73 147 T ■fV-r 40.20 40.40 40.60 40.80 41.00 5000 m/z 281.10 30.27% 231 45 369 117 207 249 I m/z-> 80 100120140160 180200220240260280300320340360380400420 Abundance #56714; i,1,1,5,7,7,7-Aeptaniethyi-3,3-bis(trimethyisiloxyjt 73 4O^2O£OAO 40.60 40.80 41.00

!■ 147 5000 267 355 429 45 207 I I I i 40 60 80 100120 140160 180 200 220 240 260 280 300 320 340 360 380 400 420 __ 40.20 40.40 40.60 40.80 41.00

4592.D GCMS0308.M Thu Mar 28 16:28:18 2002. Page 6

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