GCMS calibration data for TCLP method, May 2002

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GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

NYC-WTC_000022930–000022937

Folder label: “GCMS X 5/8/02 A 5/10/02”

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Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY0302\9568.D Vial: 42 Acq On 5 May 2002 8:11 am Operator: Sample GC/MS SCAN 4/23 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.79 4.93 ug/1 454504 Naphthalene-d8 15.83 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 3 Benzoic acrid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 000541-02-6 068595-79-9 003789-85-3 37 (9 4 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 33 Abundance Scan 1064 (14.791 min): 9568.D (-) m/ z 73.10 100.00%! 73

5000 267 355 0 45 251 14.40 14.60 14.80 15.00 15.20 I I, 89 108125 154 177193208223 -1 1 293 323339 t ‘‘111111:17 ‘111111111111271111110"EOTTETTTIUIT ITi I'1'' I " " 111111 ' ‘' l’l1111111 m/z 267.05 29.27% mfz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 ,......................................... 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 26.19%| ■ ■■ i ■ i ′ ■'■।■■ ■ ■ । ■ ■ > > । " i ■ ■ ■ ■ i 191207 i11 ■ • i ■ M ■ i 2511 i'11111 111 323339 i ' ■ ' ■ i ■' ■ ■ ■ 'i ■ 1 IIs mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73

14.40 14.60 14.80 15.00 15.20 267 m/z 356.10 9.18%| 5000 179 356 45 147 I 209 237 , |, " i ■'"' i " ■'11 ■' ‘11' ‘ “ i " " i ‘'''" i' " ' l' ‘ " i 312 341 h ' i'11 r i111111 11111' ' i " " i ■ " ' i'" TTur miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #72298: Benzoic acid, 2-[(trimethylsilyl)oxy}-, trimethylsi 1.rT 1 1 M ' m 1)11 73 267 14.40 14.60 14.80 15.00 15.20 m/z 74.10 8.45%

5000

135 47 ,i 175 193209 233249 " i' " ' i " '11 ■'1 ■ i ■1 •' i " " i' " ■ i ■ " 'f111111" 1111111 TT 1 * 282 ......................... ........................ /z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

9568.D GCMS0501.M Tue May 07 15:00:00 2002 Page 2

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GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

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