GCMS sample analysis results for unknowns, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY0802\9580.D Vial: 17 Acq On 9 May 2002 2:13 am Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

14.80 5.55 ug/1 437225 Naphthalene-d8 15.82 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 (80 2 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 3 Benzoic acid, 2,6-bis (trimethylsil 370 C16H30O4Si3 003782-85-2 33 4 N-(Trifl/oroacetyl)-N,O,O',O' 1-tetr 553 C22H42F3NO4Si4 000000-00-0 25 Abundance Scan 1065 (14.796 min): 9580.D (-) m/z 73.10 10 0.00%l 73

5000 267 355 1 ....................... । । i> > । ..................... । r til 1 । । । । i । । । । । r

45 14.40 14,60 14.80 15.00 15.20 । 1, 108 133 154 177193 223 2511 1 293 323339 1 ‘I’’ I, । i t i rT11 pi r i i" । i--r i । । । । T i । it । । । । । । । । । i T i | i I i i । F । i i । i i i i । i i i i । i i i T । r i T TT m/ z 2 67.05 35.45% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 - 5000 1440 14.60 14.80 15.00 15.20 m/z 355.10 33.57%

T9t r '1 ■ i ■ ■ ■ ■ i1111 r ■1' i' ■111 191207 TTTT Tr’ I ‘T‘ 1 1 251 1 323339 TTTT |’ ’ 1 1 A /z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet 73

Tr 14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.10 12.43% 45

133149 193 , 223 , 281 340 | 370 TI‘ TT DT7" I i1 ■ ■111'1' [ I1I i, I ’14 I I I I I IJ I I I I I II I I 0/0 I’TI’IIi

lz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet 73 355 14.40 14.60 14.80 15.00 15.20 m/ z 2 68.05 9.18%| 5000

147 267 47 .................... i li.......... 208 249 204 TTTT i. i., 11 -03 11111:1111100101 r 11 ■ i 370 ।1'" । ' 1 1 1 JY.................. ii । । n । । । । । 1 । i ~i

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

9580 .D GCMS0507.M Fri May 10 08:22:12 2002 Page 2

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