GCMS analysis results for sample AE09334, May 2002

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Data File C:\HPCHEM\1\DATA\MAY0802\9334 .D Vial: 21 Acq On 9 May 2002 6:09 am Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 14.79 9.42 ug/1 692783 Naphthalene-d8 15.83 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 72 2 Phenethylamine, N-methyl-.beta . , 3,4 399 C18H37NO3Si3 010538-85-9 38 3 Benzeneacetic acid, .alpha.,4-bis[( 326 C15H26O4Si2 055334-40-2 37 4 Benzoic cid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 Abundance Scan 1064 (14.794 min): 9334.D (-) m/ z 73.10 100.00% 73

5000 267 355 _____________ 45 14.40 14.60 14.80 15.00 15.20 1 1, 89 108125 154 177193208223 251 1 293 323339 I 0 119011010100**000700000 । r । t"i i । । । i ii । i'i । i 11 ( । । । ri r । । । i ( । । । । ■ । । । । । i । ] । । । । 1‘ । । । m/z 267.05 34.07% mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/Z 355.10 31.66% 191207 251 | 323339 | 1' r '11 r y-t > ri lt-i-q TTT -PPPPT 1 I ■' ' ' 1 I ' 1 1 U 1 ' m/z->_____ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 70 14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.10 11.50 44

IL88 130147 193 267 111piI I I I I I I I I I I I II iif । । । ii r i । । । । । । । । f । I । । । । । । । । । । ( i । । । । । । । । i i i i [■ 294 i r ] । । i i । r i i i । i' i i T' । i i

m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #46278: Benzeneacetic acid, .alpha.,4-bis[(trimethylsilyl)o .. 73 14.40 14.60 14.80 15.00 15.20 267 m/z 268.05 9.20%

5000-

89 151 179 ..... ....... ............. 1.194 I I I I I I I I I t I I I I I I I I I I I I j t I I I I I 1 I I I I t I I [ I I r I I I I I 237252 .283 311 । । । । । । । । । I I | It i i | I i i 1' 11'111111111' 111 .... / miz- 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

9334.D GCMS0507.M Fri May 10 08:21:43 2002 Page 3

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