GCMS calibration data for TCLP method, May 2002

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GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

NYC-WTC_000022953–000022960

Folder label: “GCMS X 5/8/02 A 5/10/02”

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Data File C : \HPCHEM\ 1 \DATA\MAYO 302\9569.D Vial: 43 Acq On 5 May 2002 9:10 am Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.80 3.35 ug/1 308015 Naphthalene-d8 15.82

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Benzoic acid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 43 3 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 40 4 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 Abundance Scan 1065 (14.797 min): 9569.D (-) m/ z 73.10 100.00%

5000 267 355 / rr 1 i ' 1 45 14.40 14.60 14.80 15.00 15.20 i I *T’111115 |, 108 133 —111111301100 154 177 193208223 251 323339 I —0u/f’mOuOTOTTT " ' 1'1 ■ i'' m/z 267.05 34.79% mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 .................................................. 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 33.03% , , 191207 251 |, 323339 1 I ' ' ' ' I ' ‘ " I ' ' ' ' I ' ' 1 1 1 ‘ 1 ‘ * I ' ' 1 ‘ I ' ‘ 1 ■ I ' 1 ’ ' I ‘ ' I “ ' ' I 1 1 1 ‘ 1 1 1 ' ' I ' * ' ■ i " " i • i'' 1’ m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #72298: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethylsi 73 267

14.40 14.60 14.80 15.00 15.20 5000 m/z 356.10 11.47%

135 47 175 123209 233249 282 ।" । “ i " " i " " i ■ " ' i‘ ■" 111111111' 111111'' 11111 " i1' " i1'1111111111 mfz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls ■ i ■ ' ' ' i ' ' 1 ' 1 1 1 1 1 I ' 1 73 14.40 14,60 14.80 15.00 15.20 m/z 268.05 8.86% 5000 355 44

m/z—> 1 Th’ 40 +88 60 130147 193 267 ' i ■ ‘111' ■'1111 " i ‘ " 1 r " ' i " " 1111' 111 " 11 " 'l rr" 11'1111 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 294 14.40 14.60 14.80 15.00 15.20

9569.D GCMS0501.M Tue May 07 15:00:13 2002 Page 2

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GCMS calibration data for TCLP method, May 2002 · Box DEP Box 18

NYC-WTC_000023055

GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

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