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GCMS analysis results for sample AD26009, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26009 conducted on December 12, 2001.

NYC-WTC_000030875–000030884

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01

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Scanned page image, NYC-WTC_000030883
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV2 001\26009.D Vial: 2 Acq On : 20 Nov 2001 1:34 pm Operator: 209 GALOS Sample : gc/ms unknown Inst GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.69 1.43 ug/1 288486 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative/ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 72 2 Acetic acid, 1,1 dimethylethyl este 116 C6H12O2 000540-88-5 64 3 3-Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 4 5-Hexen-2-one / 98 C6H10O _______ 000109-49-9 9 Abundance Scan 288 (7.685 min): 26009.D (-) m/z 42.95 1 00.00% i 43 I

5000 59

101 7.40 7.60 7.80 8.00 69 ll 83 "r TPTHTTIT ।...11।।> r111।11 < । I” "I' 207 m/ z 59.05 43.26% m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200210 'Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- I 43

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 20.97% 27 101 l | 83 m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200210 'Abundance #3292: Acetic acid. 1,1-dimethyletnyl ester I 43

7.40 7.60 7.80 8.00 5000 57 m/z 58.05 16.73% 101 15 27 ■ ■ I " i" " i" " I" " i" " r "' r "1 r "' i ‘' r "' i" " i" " i" " I" " i" " i" " I ‘' i" " 111" I" " 111111"' 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #1691: 3-Hydroxy-2-pentanone 1 ■ ■ । । ■ i ■ ■ ■ ■ r ■ ■ ■ ■ 31 59 7.40 7,60 7.80 8.00 m/z 41.05 6.93% 5000 - 45

I m/z-> .L.15 73 84 102 ’•r •••!" ‘‘I‘‘TTTT • • l ■ •1 I"'' i" r'" r "' r'" i" " i" " r "' r' ■' i TTTT ''1111'' I'1111111TITTTTT ' । 10 20 30 40 50 60 70 80 90 100110120130140150160170 180190 200 210 7.40 7.60 7.80 8.00

26009.D NP103001.M Tue Dec 11 09:21:07 2001 Page 1

NYC-WTC_000030883

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NYC-WTC_000030883Source: NYC Law Department, mirrored locally

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NYC-WTC_000030679 · Box DEP Box 21

Gas chromatography-mass spectrometry scan record from late October to November 2001 regarding environmental sample analysis.

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