GC/MS analysis report for sample AD25736, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\NOV1601\25736.D Vial: 23 Acq On : 17 Nov 2001 12:30 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ****************************************************************'**'*** Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.68 2.43 ug/1 389971 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Teritative ID MW MolForm CAS# Qual 1 2-Pentanone,/4-hydroxy- 4-methyl- 116 C6H12O2 000123-42-2 72 2 Acetone / 58 C3H6O 000067-64-1 12 3 Morpholin^ 4-methyl- 101 C5H11NO 000109-02-4 9 4 5-Hexen-:^one 98 C6H10O 000109-49-9 9 Nxjndance ® Scan 287 (7.678 min): 25736.D (-) m/z 43.00 100.00%

5000 59

101 7.40 7.60 7.80 8.00 V-r ' I'''' I ■ I''' ■ I''' ■ I' I I ' ■ • ■ I m/z 59.05 45.97% TiZz-> 10 20 30 40 50 60 70 80 90 100 110 WxiTKtence #64275:2-Pentanone, 4-hydroxy-4-nwthyl- 43

5000 ........ 59 7.40 7.60 7.80 8.00 m/z 100.95 19793% 15 31 101 I, I j , ,1, , [ I I iii |li , I I I I 83 ' ' 'I ' ‘ I ' ' ■ ' I ' ' '■ I ' nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62322: Acetone

' ' ' ' I ‘ ' I ' ' ' ' I ' •' 7.40 7.60 7.80 8.00 5000 m/z 58.05 19.52% 58 —rT-rT-j*i-1-r-T-y-i4^T-^^ 27 -t-r-r-p n/z-> 10 20 30 40 50 60 70 60 90 100 110 Mnindance #1640; Morpholine. 4-niethyl- 4(3 7.40 7.60 7.80 8.00 m/z 41.00 7744% 5000- 101 15 I 27 > * '■ I ■ “ ' I I r-j—r-TT—i—p ■nfe-> 10 20 30 40 50 60 70 80 90 100 110 " ' 7.40 " 7.^ ’ ' 7.M “ ioO

25736.D NP103001.M Thu Nov 29 09:21:27 2001 Page 2

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