GCMS analysis report, Sample AD26163, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26163.D vial: 60 Acq On : 1 Dec 2001 12:28 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params s LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

11.56 0.56 ug/1 121782 1,4-Dichlorobenzene-d4 11.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 64 2 Benzene-1, 2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Acenaphthy lene 152 C12H8 000208-96-8 14 4 Vanillin 152 C8H803 000121-33-5 9 Abundance Scan 710 (11.561 min): 26163.D (-) m/z 149.90 100.00% 150

5000 115 52 78 TTOTTITTTTTTTT 11.20 11.40 11.60 11.80

miz-> 30 1 ‘ 11 -+ T ------- 40 .1 40 87 I 50 IIPPPT 60 tT 70 80 90 100 110 120 130 140 150 ' ' I ‘ 160 m/z 151.90 54.16% Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 i | J : » : । : k i : j : : 1 : j I i 1 I | T

78 11.20 11.40 11.60 11.80 52 m/z 114.90 t 35.34% 35 87 -- || i 77 । > i j ।. ‘ i ‘ miz-> 30 40 50 607 '70 80 90 100 110 120 130 140 150 ■ 160 * Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 1 1 1 1 • ' TOT—um BBBnn 115 1120 11.40 11.60 11.80 5000 52 78 m/z 78.05 20.30%

35 87 ,. ।।pI_______ _......... , “111 | 1 ■ । •1111'' i1 ‘' i' ■1 • i ■ ■' ‘ i1' +.... . 1111 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #67015: Acenaphthylene T-p-r-r-r-p-r 11 n T111' 152 11.20 11.40 11.60 11.80 m/z 52.00 17.45% 5000

76 63 126 87 98 miz—> — T #— 30 —H TIBBIIOB—puur •>I• 40 50 60 70 80 90 100 110 120 130 140 150 160 । ■ 1' ‘1' i ■' ■ ‘ i ‘ ■ 1 » I I I J I j ) l * » I » 11.20 11.40 11.60 11.80

26163.D NP112601.M Mon Dec 03 12:19:13 2001 Page 2

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