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GCMS analysis results for sample AD25263, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD25263 conducted on November 28, 2001, noting unknown compounds.

NYC-WTC_000069484–000069494

Folder label: “GCMS Scan X 10/23/01 An 11/9/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0801\25263.D Vial: 4 Acq On : 9 Nov 2001 3:11 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 3.86 ug/1 718051 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, . hydroxy - 4 -methyl - 116 C6H12O2 000123-42-2 38 2 3-Hydroxy-2xp entanone 102 C5H10O2 003142-66-3 9 3 Acetone 58 C3H6O 000067-64-1 9 4 5-Hexen/2-one 98 C6H10O 000109-49-9 9 Abundance 7 Scan 288 f7.691 min): 25263.D (-) m7z 42.95 100.00% 4(3

59 5000

101 7.40 7.60 7.80 8.00 69 83 I I ‘ ‘ I ' ' ' ‘ I ' ' ' ' I ' m/z 59.05 52786% Ti/z-> 10 20 30 40 50 60 70 80 90 100 110 ^bundance #64275; 2-Pentanone, 4-hydroxy-4-methyl- 4(3

5000 59 __V40__7;60_7;80_a00___ m/z 101.05 23.18%

10 15 I 20 30 31

40 50 60 83 ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 70 80 90 100 101

110 (1 Abundance #1691:3-Hydroxy-2-pentanone 31 59 ................. 7.40 7.60 7.80 8.00 5000 m/z 58.05 17.61% 45 15 , . I.. II.. 1 ' ' ' ' I ‘ ' I ' ' ' ' I l| , I P , , I . ..... I ■ I

•n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62322: Acetone .............. / 4(3 • 7.40 7,60 7.80 8.00 m7z 41.0,0 7725%

L 5000 58 27 —Pr-r-1 I I I '■ I ■' I . . . .' I ■ I T-r-r-r-r ■nfe-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

25263.D NP103001.M Tue Nov 27 11:03:48 2001 Page 2

NYC-WTC_000069493

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NYC-WTC_000069493Source: NYC Law Department, mirrored locally

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