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GC/MS analysis results for sample AD22582, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22582 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087250–000087273

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087258
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22582.D Vial: 10 Acq On : 28 Sep 2001 9:15 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 6.38 0.42 ug/1 53564 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanone 100 C6H12O 000589-38-8 91 2 Butar^, 2,2-dimethyl- 86 C6H14 000075-83-2 53 3 3-Pe/tanone, 2-methyl- 100 C6H12O 000565-69-5 53 4 3-HXptanone, 4-methyl- 128 C8H16O 006137-11-7 45 <\bundanci Scan 146 (6.384 min): 22582.D (-) m/z43.05 100.00%

71

5000 100

85 6.00 6.20 6.40 6.60 6.80 TTTTpTrp m/z 56.95 99.28% Ti/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Sundance #63358: 3-Hexanone 4|3 57

5000 71 6.00 6.20 6.40 6.60 6.80 100 m/ z 71.00 65.23% t I"' I l.l III.•Ill 111 ll 11" n 1111111 'I..... . TiZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #732: Butane, 2,2-dimethyl- 43 517 71 6.00 6.20 6.40 6.60 6.80 29 m/z 100.05 35.86% 5000

nZz-> Abundance ,0^ 15 r'" r' “ I + 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #63398:3-Pentanone, 2-methyl-

43 5(7 'k JL 6.00 “mTz 6.20 41.05 6.40 6.60 28797% 6.80

5000

n/z-> I" ''I'"‘ I"''I" "I -YY. 71

......... I...... 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 85 I"'' I" ‘ 'I" I'"' I 100 kSxAl 6.00 6.20 6.40 6.60 6.80

22582.D NP091101.M Wed Oct 03 12:08:58 2001 Page 1

NYC-WTC_000087258

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