Gas chromatography-mass spectrometry analysis of sample AD24482 completed November 13, 2001, identifying other unknown compounds with violations referenced in comments.
NYC-WTC_000068748–000068762Folder label: “GCMS Scan X 10/15/01 A 11/3/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24482.D Vial: 21 Acq On : 3 Nov 2001 10:28 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.41 1.09 ug/1 154813 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 2-Hexanone 100 C6H12O 000591-78-6 90 2 Methyl leobutyl Ketone 100 C6H12O 000108-10-1 58 3 2-Hexaifone, 4-hydroxy-5-methyl-3-pr 172 C10H20O2! 061141-74-0 45 4 2-Hexanone, 4-methyl-______________ 114 C7H14O 000105-42-0 39 Abundance Scan 149 (6.414 min): 24482.D {-) m/z 42.95 100.00% 40
58 5000
71 85 100 Too^ 6.20 6.40 6.60 6.80 |l"q-........ I..... m/z 58.05 58.85% Tiy2-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ^bundance #63386:2-Hexanone 43
........................................... 5000 58 6.00 6.20 6-40 6.60 6.80 29 m/z I 71 85 ^00 I" '' I' 111 r " ' I" " 11" ' I' " ' I " " I" " I " " I"'' I" " I'' " I ■nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63351: Methyl Isobutyl Ketone 40 6.00 6.20 6.40 6.60 6.80 5000 m/z 41.05 14.53% 58 27 85 100
Tife-> I..... ,^1...... 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #15807:2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 40 6.00 6.20 6 40 6.60 6,80 m/z 99795 11.76%
K, 5000 58 27 100 '"pUj............ lyrrTTp- ' I' <" I"' 1^-1 ■ Tlfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60 6.80
24482.D NP103001.M Fri Nov 09 14:54:31 2001 Page 2
NYC-WTC_000068757
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000068763
Laboratory report documenting GCMS analysis of sample AD24483 identifying unknown compounds on November 13, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068529
Laboratory report documenting GCMS analysis of sample AD24480 conducted on November 14, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069587
Laboratory report documenting GCMS analysis of sample AD25377 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068447
Laboratory report documenting GCMS analysis of sample AD24473 conducted on November 9, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068572
Laboratory report documenting GCMS analysis of sample AD24487 conducted on November 13, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068585
Laboratory report documenting GCMS analysis of sample AD24488 conducted on November 13, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068634
Laboratory report documenting GCMS analysis of sample AD24492 conducted on November 13, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068893
Laboratory report documenting GCMS analysis of sample AD24730 identifying unknown compounds on November 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067675
DEP lab report for GCMS analysis of sample AD23948 conducted on October 25, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067796
Laboratory report documenting GCMS analysis of sample AD23998 conducted on October 29, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067752
Laboratory report documenting GCMS analysis of sample AD23995 conducted on October 29, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089461
Laboratory report documenting GC/MS analysis of sample AD23833 conducted on November 1, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000068720
Record of a GCMS scan conducted at the World Trade Center site in mid-November 2001.
Filed in the same folder
NYC-WTC_000068721
Document page containing identification codes for GCMS scans conducted in November 2001 within DEP Box 60.
Filed in the same folder
NYC-WTC_000068724
Instrument data sheet containing operational parameters and sample details for GCMS analysis conducted on October 15, 2001.
Filed in the same folder
NYC-WTC_000068737
Laboratory report documenting GCMS analysis of sample AD24333 with detection of unknown compounds on November 27, 2001.
Filed in the same folder
NYC-WTC_000068763
Laboratory report documenting GCMS analysis of sample AD24483 identifying unknown compounds on November 13, 2001.
Filed in the same folder