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GCMS analysis results for sample AD24052, Oct 29 2001

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Laboratory report documenting GCMS analysis of sample AD24052 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067894–000067907

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\24052.D Vial: 13 Acq On : 26 Oct 2001 12:25 am Operator: 209 GTVLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Paramss LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.36 0.46 ug/1 88529 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanone 100 C6H12O 000589-38-8 72 2 3-Pent^one, 2-methyl- 100 C6H12O 000565-69-5 40 3 Pentarfe, 3-bromo- 150 C5HllBr 001809-10-5 32 4 3-He; anone, 4-methyl- 128 C8H16O 006137-11-7 28 Wiundance ■ Scan 143 (6.360 min): 24052.D (-) m/z 43.00 100.00% 4i3 57 71 J 5000 IO)

6.00 6.20 AJ 6.40 6.60 6.80 85 m/T 57.00 95.92% TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #63358:3-Hexanone 43 57

71 5000 6.^' ‘ 6.40 “ 6.CT “ 6.80 6.00 100 m/z 71.00 68.77% W-rpYtVi-r n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #63398: S-Pentanone, 2-methy)- 517 43 6.00 6.20 6.40 6.60 6.80 5000 m/z 100.05 42.83% 100 71 85 T-p-m-p’ n/z-> 20" ’ M 50 60 70 80 90 100 110 120 130 140 150 Abundance #9587: Pentane, 3-bromo- 43 71 6 00 6.20 6.40 6.60 6.80 m/z 41.05 30.99% 5000 27 55

108 150 ' I "I' I' '■p 111111111 • I'''' 1 I'''' I '''' I Tl&-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 6.00 6.^ 6.^ 6.OT 6,80

24052.D NP101901.M Fri Oct 26 10:32:05 2001 Page 1

NYC-WTC_000067902

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NYC-WTC_000067902Source: NYC Law Department, mirrored locally

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