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GCMS analysis results, sample AD24048, October 29, 2001

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Gas chromatography-mass spectrometry analysis of environmental sample AD24048 conducted on October 29, 2001, identifying unknown compounds.

NYC-WTC_000067840–000067854

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\OCT2501\24048.D Vial: 9 Acq On : 25 Oct 2001 8:30 pm Operator: 209 GALOS San^le : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.70 0.58 ug/1 97566 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexan61 102 C6H14O 000626-93-7 83 2 2-Peiil<anol, 4-methyl- 102 C6H14O 000108-11-2 83 3 2-P^tanol, 3-methyl- 102 C6H140 000565-60-6 56 4 2-^xanol, (S) - 102 C6H140 052019-78-0 40 Scan 181 (6.702 tnin): 24048.D (-) Wz 44795 100.00% 40

5000

41 69 6.40 6.60 6.80 7.00 , 51 F® m/z 41.05 16.86% tt/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584:2-HexanoI 43

5000 ' 'a^‘ ‘a^' 6.^ ‘7.^' "m/z 69.0,0 16.45% 19 y.31 4^1 iiini.l.'lilitrTqnTii.lH ....... ....... TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546:2-Pentanol. 4-methyI- 40

6.40 6.60 6,80 7.00 5000 m/z 44.00 11.93%

27

nfe-> 19 J 31 UIJ•<tpI>III< <II 42 T 8487 "I...... I' 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1777:2-Pentanol. 3-methyl- 40 ' 'e.^' 'aM* zro m/z ,43.00 11714% 5000

41 56 27

■nfe-> X ............. .t ‘ 1" '' I ■ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

24048.D NP101901.M Fri Oct 26 10:21:00 2001 Page 4

NYC-WTC_000067851

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NYC-WTC_000067851Source: NYC Law Department, mirrored locally

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