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GCMS analysis results for sample AD24134, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24134 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067922–000067935

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\OCT2501\24134.D Vial: 15 Acq On : 26 Oct 2001 2:22 am Operator: 209 GALOS Sample : gc/ms unknown Inst t GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method s C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.70 0.52 ug/1 82831 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-He: .ol 102 C6H14O 000626-93-7 83 2 2- .^..tanol, 4-methyl- 102 C6H140 000108-11-2 83 3 XHexanol, (R)- 102 C6H14O 026549-24-6 64 4 -Butanol 74 C4H10O 000078-92-2 50 Abundance Scan 181 (6.702 min): 24134.D (-) m/z 44795 100.00% 4)5

SOW -1. yrr,. I,, ■. 41 69 8487 6.40 6.60 6.80 7.00 I ‘‘ I''' ‘ I " ' ‘ I'' " I .i-i..................... 1,72 ■ 11 1 111..,.. I "1,... '' I' I" 1" " I in/z 69.00 15.38% Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ^bundance #63582:2-Hexanol 4b

5000 A 6.40 6.60 6.80 7.00 27 m/z 41.00 10.88%

•nZz-> Abundance 19 ■ 31, ,ii 4 I 8487 ' I " " I "'' I" “ I' * ‘' 11"' I ‘' I' m I' I" " I' I'' I ‘" I ‘" 11 “ " I" " I" '' I ‘ I" I"'' I “ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 69

#63547:2-Pentanol, 4-methyl-

6.40 6.60 6.80 7.00 5000 m/z 43.00 10.19%

27 69 I ■ •' ■ I ■ I > > I ■ > •' I 38 42 ) 8487

.AJL^.. * I ' • ' I • • • • I • ’ ' ’ I • ' » » I ' • • ' J ” ' ' I • • ’ • I » • ” ) ” » « I H 1 I I • I I I I I I U I » n » I I I I I I I n I I I I I > I J in J I I nfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1794:2-Hexanol. (R). - ?-(I I I I I ■ I I I i I I-1"! I 4)5 6.40 6.60 6.80 7.00 in/z 44.00 8772% 5000

69 .. 19.. 1?..........55 .... .............. 8487 10 1 5 20 25 TO 74'^"^ ' 6.^ ' ' ‘ 7.00

24134.D NP101901.M Mon Oct 29 09:33:51 2001 Page 3

NYC-VVTC_000067932

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NYC-WTC_000067932Source: NYC Law Department, mirrored locally

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