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GCMS analysis results for sample AD24134, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24134 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067922–000067935

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File s C:\HPCHEM\1\DATA\OCT2501\24134.D Vial: 15 Acq On : 26 Oct 2001 2:22 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : Cs\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.45 0.91 ug/1 145587 1,4-Dichlorobenzene-d4 11.73 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanipne 100 C6H12O 000591-78-6 91 2 2-He: one, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 83 3 Oxiri .ne, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 72 4 M^hyl Isobutyl Ketone 100 C6H12O 000108-10-1 58 igwpgfinee Scan 154 (6.454 min): 24134.D (-) m/z 43.00 100.00% 43

58 5000

' ' ' ' I ' ' ' ‘ I ' ' ' I ' ' ' ' I 85 100 6.20 6.40 6.60 6.80 50 Wtv J. ^1 71 L I. ‘ I ' ' ' ' I ' ' ' ' 1 ' m/z 58.05 56.65% m7z~> 20 30 40 50 60 70 80 90 100 110 120 130 140 Sundance #63386:2-Hexanone 43

5000 58 29 “m/z 577^0 19.24% I.. J” ■ Tife-> 20 30 40 '50'' ‘ ‘ '70 " TO ‘ 90 “iro' iio‘w' ‘i40 Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43 58 6.20 6.40 6.60 6.80 5000 29 “mTz 41.05 17.48%

TiZz-> ' 1 ''' ‘ I' • ‘ ' I ' 20 30 40 ,1, ‘ I' ‘ 50 60 ' I ‘ 71... 140 70 80 90 100 110 120 130 140 Abundance #1530: Oxitane, 2-methyl-2-(1-m^ylethyl)- 40 ‘ ' 6.^ " 6.CT " 6.OT " 58 m/z 100.05 11.90% 5000 I 71 30 85 100 ' '|~ “'ll >’1 • • * • I' mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.:a3 6.40 6.60 6.80

24134.D NP101901.M Mon Oct 29 09:33:48 2001 Page 2

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NYC-WTC_000067931Source: NYC Law Department, mirrored locally

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