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GCMS analysis results, sample AD23994, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23994 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067705–000067719

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23993.D vial: 17 Acq On : 18 Oct 2001 4:53 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.50 ug/1 46432 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanol X 102 C6H140 000623-37-0 83 2 3-PentanoZ 88 C5H12O 000584-02-1 36 3 2-Propasrol, 2-methyl- 74 C4H10O 000075-65-0 33 4 3-Peqtanol, 2-methyl-______________ 102 C6H14O 000565-67-3 25 'Abundance < Scan 172 (6.617 min): 23993.D (-) m/z 59.05 100.00% 55

5000 73 43 , [ , J ■ . I . .

39 6,20 6.40 6.60 6.80 7.00 84 -rrnrr m/z 54.95 74.03% TiZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ^bundance #63531:3-Hexanol

55

5000 73 6.20 6.40 6.60 6.80 7.00 43 Wz 737^5 46.16% 39 I ”’‘I +W-T +4 11" " I" “ I “ " I TTfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #851:3-Pentanoi 5b 31 6.20 6.40 6.60 6.80 7.00 5000 m/z 43.00 30.98% 27 41 15 An AJ T-A I ‘“ I “ ’' I" " I" " I " “ 1"' ‘ 1 'nfe-> 5 10 15 20 25 30 35 40 45 50 55a)65 70 75 80 85 90 Abundance #62575:2-Propanol, 2-methyl- 5b 6.^' 'qM 6.OT 6.80 '7.00' “m/z 41.05 21.52%

5000 31 41 15 27 38 44 56 tA 1 b 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 6.^ ’ ' 6.40 ' ' 6.OT ' ' 6.80 ' ' 7.00' ■nfe-*

23993.D NP101901.M Wed Oct 24 11:23:22 2001 Page 3

NYC-WTC_000067715

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NYC-WTC_000067715Source: NYC Law Department, mirrored locally

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