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GCMS analysis results for sample AD24488, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24488 conducted on November 13, 2001, identifying unknown compounds.

NYC-WTC_000068585–000068597

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV0 501\24488.D Vial: 6 Acq On 5 Nov 2001 4:50 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.43 0.72 ug/1 123617 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 7 100 C6H12O 000591-78-6 91 2 Oxirane, 2>methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 78 3 Methyl I^utyl Ketone 100 C6H12O 000108-10-1 58 4 PentanaX 2,4-dimethyl-_____________ 114 C7H14Q 027944-79-2 45 Abundance Scan 151 (6.428 min): 24488.D (-) m/z 42.95 100.00% 43

58 5000

71 85 100 6.00 6.20 6.40 6.60 6.80 51 ■■■I............. I.......... m/z 58.05 56.92% Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556: 2-Hexanone 43

58 5000 — •"l ' ' ' ' I ' ' ' ' I ' ' ''I ' ’ ' 6.00 6.20 6.40 6.60 6.80 m/z 57.00 18.16% 27 85 100 71 ..... I'l............. . ■In........ ..................... 111" 111111 TTfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Waundance #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 4)3 58 6.00 6.20 6.40 6.60 6.80 5000 “inTz 41.05 17.96% 71

30 66 85 100 ........ .............. 'I n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63351: Methyl Isobutyl Ketone 4)3 6,00 6.20 6.40 6.60 6.80 m/z 100.05 9.42%

5000 58 27 85 100 p " ' I' I'«1' " ' I i72........ 1........... 1........ +t tU ,,,,,, TTfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60 6.80

24488.D NP103001.M Fri Nov 09 12:11:13 2001 Page 1

NYC-WTC_000068593

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NYC-WTC_000068593Source: NYC Law Department, mirrored locally

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