GCMS analysis comments for sample AD28669, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC0401\28692.D Vial: 19 Acq On : 5 Dec 2001 5:56 am Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1-Heptadecanol, acetate Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 29.69 0.69 ug/1 122495 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Heptadecanol, acetate 2 Acetic acid, octadecyl ester 3 1-Octadecanol 4 17-Pentatriacontene 298 C19H38O2 312 C20H40O2 270 C18H380 491 C35H70 000822-20-8 000822-23-1 000112-92-5 49 006971-40-0 47 99 Abundance Scan 2684 (29.685 min): 28692.D (-) m/z 43.05 100.00% 43

83 5000 61 97 111 —AA=.— mz—> — 40 —lullll A I — -.— 60 80 125 139 153 207 224 252 11’2’011117001—IT—IITr 100 120 140 160 180 200 220 240 260 280 300 29.40 29.60 29.80 30.00 m/z 83.05 56.27% Abundance #42500:1-Heptadecanol, acetate 43

5000 61 83 97 - U AA 29.40 29.60 29.80 30.00 m/z , 55.00 48.72%

miz-> 40 L.:o 60 80 T 210 I • 238 I ' I'''' ■ I 100 120 140 160 180 200 220 240 260 280 300 298 11" "I । " 11'

A #73049: Acetic acid, octadecyl ester 43

83 97 29.40 29.60 29.80 30.00 5000 m/z 97.00 45.90% 61 111 125 [ 139153 224 252 miz-> Abundance -r-n-p-r 40

43 57 60 80

83 1TIT । ■ ■ ■ ■ । -fTT-rrpT-n T’TTTTTIIr 100 120 140 160 180 200 220 240 260 280 300

97 #72029:1-Octadecanol A ' ■ i ' ' ‘ ' i ' 29.40 29.60 29.80 30.00 m/z 61.05 43.51% 5000 70 111 125

m/z—> ’ 1—4 IT 40 60 80 X I,, .. .... ... 224 252...... 100 120 140 160 180 200 220 240 260 280 300 A T’T , TTITETTTE’T’ 29.40 29.60 29.80 30.00

28692.D GCMS1126.M Thu Dec 06 12:39:29 2001 Page 3

NYC-WTC_000035016