GCMS analysis comments for sample AD28669, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC0401\28692.D vial: 19 Acq On : 5 Dec 2001 5:56 am Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Heptadecane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 30.63 0.58 ug/1 102087 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heptadecane 240 C17H36 000629-78-7 (9 1 2 Tetracosane 338 C24H50 000646-31-1 9 3 Docosane 310 C22H46 000629-97-0 9 0 4 Octadecane ___________________ 254 C18H38 000593-45-3 86 Abundance Scan 2787 (30,631 min): 28692.D (-) m/z 57.00 100.00% 57 43 71 85 5000

99... TLT

m/z-> T UI 40 60 4 30.60 11127141155 182 207........................... m/z 71.10 i i !j i i T i । ii i i | l i li | t ii i |i i i t | i i i IT’’ I I | I I I I | > I

260 280 300 80 100 120 140 160 180 200 220 240 | I III | > I > I | I I I > | .

320 340 30.40 30.80 31,00 72.12% Abundance #32063: Heptadecane 57 71 85 5000 GPTTTArr {r e' 30.40 30.60 30.80 31.00 99 m/z 43.05 69.65% . ............................... '' i'' mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71 —TPITTfi 30.40 30.60 30.80 31.00 5000 85 m/z 85.05 53.27%

1 113127 155169183197 294 338

mlz-> M 40 60 80 100 120। 140।.A160।. r..180। X।। d rr r i ■ ........... .. 200 220 240 260 280 300 320 340 Abundance #44318: Docosane P4Ar - —4 — , . । । . । 57 30.40 30.60 30.80 31.00 71 m/z 41.00 31.24% 85 5000

99

m/z—> 40 “ p 60 1’127141155169— I I r( I ! | I I Ti | i l . > | ! I I I | > ! I I | I i I ' i"■ ■ i " 80 100 120 140 160 180 200 220 240 260 280 300 320 340 266 310 i ■ ■ ■ ■ i " " i ■ ■ ■ ■ i " 1 ■ i ■'1 ■ r MAAWAAMMMCYAAA 30.40 30.60 30 80 31.00

28692.D GCMS1126.M Thu Dec 06 12:39:31 2001 Page 4

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