GCMS analysis results for sample AE07490, April 2002

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DEP laboratory report showing GCMS analysis results for sample AE07490 conducted on April 23, 2002.

NYC-WTC_000047137–000047146

Folder label: “GCMS X 4/1/02 A 4/20/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\APR1802\7490.D Vial: 23 Acq On 20 Apr 2002 3:01 pm Operator: Sample gc/ms scan 4/1 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Heneicosane Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 34.15 0.44 ug/1 57106 Chrysene-dl2 33.64 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 74 2 Nonacosane 408 C29H60 000630-03-5 72 3 Hexacosane 366 C26H54 000630-01-3 72 4 Eicosane, 9-octyl-_______________ 394 C28H58 013475-77-9 72 Abundance t Scan 3170 (34.145 min): 7490.D (-) m/ z 57.00 100.00% 57

85 5000 227 WAAM/AAA/AA/

m/z-> a’l i" " i111111 mH 208 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 400 281 J_________ I______________ ir" r i" " I1111 r 1 H i " " i I’III’II’I 1' f■111T11'1।1111 nfy i 1

m/z 33.80 34.00 34.20 34.40 71.00 76.04% Abundance #42201: Heneicosane 57

85 5000 ' A MW___ _ AAA A A ' ' I ' ‘ ' I 1 ' ' ' I 1 11 1 1 13 I 1 33.80 34.00 34.20 34.40 m/z43.05 72.62% 113 4 1.1141....... I' n ' I1 11 'T' 111111" . fl । i'i 11 111 111 j 11 268 296 i " 1' i "111' H 11' "1 r1" i11'11111111111111111" " I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #54526: Nonacosane 43 WANWA I I I 1_ f I I I I I I Wony I I I I I I I I I I I I I I

71 33.80 34.00 34.20 34.40 5000 m/z 84.95 54.05%

I i 99 127 ■I l , 211 239 379 408 ‘ ‘I r ■" i ’ " "i ■ 1‘110—E110EUTTI"TEI1""‘‘T

A___ " i1" ‘ r1111'1" i" " i 1111 '11I"1111'111 n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #51010: Hexacosane 1 1 1 1 11 ’ I ’ 1 1 1 I ’ 1 1 r l 1 1 1 1 57 33.80 34.00 34.20 34.40 m/z41.05 33.19% 5000 85

m/z-> .113 141 ii 169 ।. n . |T>. i-| । in । ii 111*11 295 T1‘31111111"‘T131111111"‘1‘11111"OETUTT‘TT 366 \ AMY AA / MAA , 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 400 33.80 34.00 34.20 34.40

7490.D GCMS0419.M Mon Apr 22 12:36:24 2002 Page 1

NYC-WTC_000047144

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GCMS analysis results for sample AE08834, April 25, 2002 · Box DEP Box 27

NYC-WTC_000049147

Laboratory report documenting GCMS analysis of sample AE08834 conducted on April 25, 2002, showing detection of unknown compounds.

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