GC/MS calibration data for sample 28322, Dec 2001

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Data File : C:\HPCHEM\1\DATA\DEC2701\28322.D vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Octane, 2,2-dimethyl- Concentration Rank 19

R.T. EstConc Area Relative to ISTD R.T.

12.51 0.50 ug/1 195535 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Octane, 2,2-dimethyl- 142 C10H22 015869-87-1 50 2 Heptane, 2,2-dimethyl- 128 C9H20 001071-26-7 47 3 Hexane, 2,2,5-trimethyl- 128 C9H20 003522-94-9 45 4 Heptane, 2,2,4,6,6-pentamethyl- 170 C12H26 013475-82-6 40 Abundance Scan 813 (12.508 min): 28322.D (-) m/z ’ 57.00 100.00%

m/z~> 5000

Abundance —TTTr — 20 30 36 । , 40 50 60 43

70I__ 80 57

90 #8097: Octane, 2,2-dimethyl- 71 85 +654141.7720011119 . 110™.120 127,, 100 130 A... I?.1 r।।1 .... 1 12.20 12.40 12.60 12.80 m/ z 56.00 45.23%

57

5000 41 ■ • i ■ > 414***I**’I***’I 12.20 12.40 12.60 12.80 71 m/z 43.05 41.42% 85

JNN i 27 1 ,1, , P PPri , +TT । 11 । । 1 retr ■ i ■ ■ ' ' i ■ ■ ■ ■ i ■ ‘ ■ 1 ■ ■ 127 • ■ i ■ ‘ m/z-> 20 30 40 50 60 70 80 90, 100 110 120 130 Abundance 66136) tleptan t - th- 57

12.20 12.40 12'60 12.80 5000 41 m/z 41.05 31.70% 71 : m/z-> Abundance 20 27 t । . . J. । ■ . . . । 1 . . 51 30 40 ■ i ' 1 ■ 1 i ■ ■ ‘ ■ i 50 57 60 70 80 113 ■ i ■ ■ ■ ■ i ■ ■ ' ' i ' ■ ■ ■ I ' 1 • ‘ i ■ 1 ■ ■ i ■ ■ 90 100 #65129: Hexane, 2,2,5-trimethyl- 110 120 130 AN12.20 12.40 12.60 12.80 m/ z 71.05 29.77%

miz-> 5000

20 30 41

40 50 60 ' ‘ 70 71 J______________ 80 90 100 110 120 * 130' 113_________ AN ‘ ‘ l r-r “ ’ I ' ■ ‘ ‘ I ' ‘ 12.20 12.40 12.60 12.80 ‘ I ‘ ' ‘ I

28322.D GCMS1126.M Wed Feb 06 12:55:48 2002 Page 3

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