Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018492–000018518Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\28322.D Vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
11.13 4.79 ug/1 1868350 1,4-Diehlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 86 2 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 3 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 4 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance - Scan 663 (11.131 min): 28322.D(-) m/z 281.00 1 00.00% 281
5000 1 ■ i ■ • ■ • i ■ f ■ ■ i ■ ■ ■ ■ i 45 59 73 89 193 119 133 147 163 177 123 297 221 235 249 265 10.80 11.00 11.20 11.40 0- TTnfumT,mmutTTHToTu/mumumTTTTToTt rr rn/z 282.00 27.77% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281
5000 ' 1 i ‘ ‘ i • ‘ ‘ ■ i ■ ■ ■ ■ i 10.80 11.00 11.20 11.40 m/z 283.00 17.13% 73 133 163 177 191 207 235 249 265 | TT—otnuu—uanmmTann!nt*tI3TT—*huhinu—tu9ut]nu——n—r miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-0x0-4-phen,-6-(4-chlcrocheny’* 1 2-dinydrcpynmi 281 1 ■ i ■ • ' ‘ i ■ ■ ■ ■ i 10.80 11.00 11.20 11.40 5000 m/z 192.90 11.40%
102 123 141 175 204 247 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 .................. ........ ...................... Abundance #39602:6,7-Benzo-phenothiazine-5,5-dioxide 281 10.80 11.00 11.20 11.40 m/z 133.00 10.83% 5000 217 232
m/z-> ■ i • ‘ ■ i ‘ ■ i1 192 118 .......... 189.204............. 252264 . 1 ■ i ■ • ■ ■ i • ■ ■ • i ■ • • • i 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40
28322.D GCMS1126.M Wed Feb 06 12:55:44 2002 Page 2
NYC-WTC_000018499
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NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
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NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
Filed in the same folder