GC/MS calibration data for sample 28322, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\28322.D Vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

7.62 1.89 ug/1 735669 1,4-Diehlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol,/3-methyl- 102 C6H140 000077-74-7 36 2 1,3-Dioxolane, 2-(1-methylethyl) - 116 C6H1202 000822-83-3 25 3 2-Methyl-X~hexen-3-ol 114 C7H140 032815-70-6 23 4 Silane, /tetramethyl- 88 C4H12Si 000075-76-3 9 Abundance Scan 280 (7.615 min): 28322.D (-) m/z 73.00 1 00.00% 73

5000 43 i ■ ' • • l ■ 87 103 7.20 7.40 7.60 7.80 8.00 --38445,57, ■, 694, —TTTmd 80 90 100 110 120 130 126 m/ z 43.05 37.32% miz-> 20 30 40 501 60 70 Abundance #63573: 3-Pentanol, 3-methyl- 73 - 5000 THTTr 55 7.20 7.40 7.60 7.80 8.00 97 45 87 m/ z 41.00 13.41% 27,39, 1...... , 1 i ■ ■ ■ • i ■ ‘ ■ • i * • • • । ■ • < ■ । ■ ■ ■ • । • । ■ i 1 ■ i ■ • ■ ■ i ■ ■ ‘ ' i ‘ ‘ ‘ ■ i ‘ ■ • ■ i ' ■

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #84281 ■ l S-Bioxolane, 2-{1 mots ir ‘y‘ ‘ 73

7.20 740 7.60 7.80 8.00 5000 m/z 44.95 11.73%

27 39 45 56 86.............. 115 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3017:2-Methyl-5-hexen-3-ol PA r mrrm mm ! ■ ■ 73 7.20 7.40 7.60 7.80 8.00 55 m/z 71.00 7.42% 43 5000 27

miz-> 20 30 40 1‘i ' l 50 1,1 1 1 ''' 1 1 1 60 70 1 80 90 100 110 120 130 —TPfrmTur 7.20 7.40 7.60 7.80 8.00

28322.D GCMS1126.M Wed Feb 06 12:55:39 2002 Page 1

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