GCMS analysis summary, sample AD31349, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JANI502\31349.D Vial: 24 Acq On : 16 Jan 2002 10:26 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.45 4.76 ug/1 1090730 1,4-Dichiorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol/ 3-methyl- 102 C6H140 000077-74-7 28 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 1,3-Dioxolane, 2-methyl- 88 C4H8O2 000497-26-7 9 _4 Pentane/ 3-methoxy-__ 102 C6H140 __ ________ 036839-67-5 9 Abundance' L Scan 262 (7.446 min): 31349.D (-) m/z 73.00 100.00% 73

5000 43 • ■ • ■ । ■ 1 1 ■ । ‘ । ’in ■ । ■ • • 38 |, 1 49 55 61 67, । , 87 103 7.20 7.40 7.60 7.80 ‘ ' I * ’ 4 • I ‘ ‘ 1 ‘ 1 '“r1 1 11 i' । 1 1 I 1 ‘■‘l| I 1 1 1 > 1*** 1 r‘I ‘‘ m/z 43.05 33 .72% m/z~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63572: 3-Pentanol, 3-methyl- 73 5000 ‘ • ■ ■ i ‘ ‘ 1* i • ' ■ ■ 14TT । । । । i 55 _ 7.20 7.40 7.60 7.80 45 __ m/z 41.05 12.28% 87 27 m/z-> 10 20 30 1 ' I H'i ' I * das 1 1 1 1 1 40____50 _ 60___ 70_ 1r > I 1 11 1 i 1 1 ■ ■ I 1 1 ' 1 I 1 80 90 100 110 Abundance 6293% S; 0 afarcth, 73 tTF. mn ■ 1 * 1 i ‘ ■ 1 1 i ■ 1 ‘ 7.20 7.40 7.60 7.80 5000 m/z 45.05 12.26% 45 15 53 59 88 1IIIIIIIII 1 1 1 1 ‘ 1 ‘ i ‘ 1 ‘ ' I ■ ■ • ‘ i ‘ ‘ ' ■ i ' ■ ■ ■ i ‘ ‘ ■ ■ i ■ ‘ ■ • i • miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902:1,3-Dioxolane, 2-methyl- 1 ■ ■ ngr r ■ /. . Tp 111 73 7.20 7.40 7.60 7.80 m/z 71.00 6.90% 5000 43 58 27 87 anpoapondIpi 41' 1 | ' 1 1 ‘ r ri i 1 m 1 1 1 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

31349.D GCMS1126.M Mon Feb 04 15:03:40 2002 Page 1

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