GCMS unknowns analysis results for sample AD28335, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN0802\28355A.D Vial: 4 Acq On 8 Jan 2002 6:13 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Octane,. l,l’-oxybis- Concentration Rank 20

R.T. EstConc Area Relative to ISTD R.T.

12.80 1.89 ug/1 605225 1,4-Dichlorobenzene-d4 11.52

Hit# of 5 Te: ative ID MW MolForm CAS# Qual

1 Octane, 1,1' 7oxybis - 242 C16H340 000629-82-3 64 2 Heptane / 100 C7H16 000142-82-5 64 3 Undecane, 2, 8-dimethyl- 184 C13H28 017301-25-6 64 4 Nonane, 2-methyl-5- propyl- __ _ 184 C13H28 031081-17-1 53 Abundance * Scan 845 (12.799 mln): 28355A.D (-) m/z 57.00 100.00%

k 57 71 43 5000 85 J I ‘ ' 1 I 1 ‘I T TIT TIr T 12.40 12.60 12.80 13.00 13.20 j miz-> 20 h. ■. .. ,. —- TTt 40 60 +99112127 141155—. .. ... 80_ 100 120 140 160 180 200 220 m/z 71.10 86.64% Abundance #71250: Octane, 1,1-oxybis- 43 57| 71 71

5000 84 12.40 12.60 12.80 13.00 13.20 27 112 m/z 43.05 68.26%

MA 97 ,h . . 143 224 ! miz-x 20 I ■ ■ ■ • l ' 40 60 W 80 TITUETT TTTTTT TTTTT । । TT. >. T 100 120 140 160 180 200 220 [Abundance #63439: Heptane 43 ! i 12.40 12.60 12.80 13.00 13.20 57 m/z 55.95 41.93%

k 5000 71 27 85 100 T——TT—T , , TTT TTTTT Tmr TTTTTTIT _ miz-? Abundance 20 i 1 ■ ' ' i 40

43 60

57 80 100 120 140 160 #18991: Undecane, 2,8-dimethyl- 180 200 220 J TTT A=— 12.40 12.60 12.80 13.00 13.20 71 m/z 41.00 40.79% 5000 85

m/z-> 27 —. — ■ + - 20 99 113 40 141 i -1 ------- 60 80 100 120 140 160 180 200 220 V, W A 12.40 12.60 12.80 13.00 13.20

28355A.D GCMS1126.M Wed Jan 09 09:09:21 2002 Page 5

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