GCMS analysis results for sample AD30352, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30352.D Vial: 19 Acq On : 28 Dec 2001 5:38 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

11.44 0.46 ug/1 147601 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 64 2 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 59 3 2-Propanol, 1-(2-ethoxypropoxy)- 162 C8H18O3 010143-32-5 39

NU 4 2-Propanol, 1,1’-[(1-methyl-1,2-eth 192 C9H20O4 _ 001638-16-0 38 Abundance Scan 697 (11.440 mln): 30352.D (-) m/z 59.05 100.00% ! 59 45 5000 73 103

11.20 11.40 11.60 11.80 311,,.51 J I 1 I I jU'!^ ■ | ■ 85 > | ITI 1 |-| ' ' l‘ ' ' ' I ‘ ' 1 I 1 ’ I1 m/z 45.05 55.97%

_, Nd miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238:2-Propanol, 1-(2-methoxy-1 -methylethoxy) 59

5000 45 73 103 11.20 11.40 11.60 11.80 ‘ 31 m/z 103.05 34.35% ............ 130. m/z-s 20 ' ‘ 30 40 50 I 60 70 *rt i 80 ■ i ■ 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3.3’oxybis- 59

11.20 11.40 11.60 11.80 5000 31 45 m/z 73.00 29.88% 103

i Abundance 20 30 40 TP———mDm2u—pu9mnegnngr 50 60 70 80 90 134 100 110 120 130 140 #12860:2-Propanol, 1-(2-ethoxypropoxy)- 59 A W OBn—mmGOgTuT 11.20 11.40 11.60 11.80 m/z 41.05 25.80%

m/z-> 5000 31

* । ■ 1 • ■ f1 ■ ■ ' । 20 30 40 45

■ ■h I r ' 50 73 103 ............. ............ ........................ . ..................... 60 ' ' Vo 80’ 90 100 110 120 130 140 _MA OIITgm 11.20 11.40 11.60 11.80

30352.D GCMS1126.M Wed Jan 02 10:50:32 2002 Page 5

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