GCMS analysis comments for sample AD29141, Dec 17 2001

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1001\29141.D Vial: 8 • Acq On : 10 Dec 2001 5:34 pm Operator: 209 GALOS Sample : gc/ms scan 11/30 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.74 ug/1 177905 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-metho: -1-methylet 148 C7H1603 020324-32-7 83 2 2-Butanol, 3,3' -oxybis 162 C8H18O3 054305-61-2 64 3 2-Propanol, 1,1‘-Oyybis- 134 C6H14O3 000110-98-5 50 4 2 ~ Propanol, 1-(2 ethoxypropoxy) - 148 C7H1603 _________ 013429-07-7 47 Abundance < Scan 695 (11.428 min): 29141.0 (-) m/z 59.05 100.00%

A 59 i l 5000 45 103 73 11.00 11.20 11.40 11.60 11.80 391 1— | . THTTtrur 85 m/z 44.95 46.76%

N i1 • ■11 ■ ■ ■ ■ । ■ ■ ■ ■ । ■ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238:2-Propanoi, 1-(2-methoxy-1 -methylethoxy) 59

5000 45 103 ur 73 11.00 11.20 11.40 11.60 11.80 31 m/z 103.00 35.05% — । । . T’ T —Ht -* __________ 130 TTIu66I1TIITIrrrTT miz->__ 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3.3’-oxybis- 59

11.00 11.20 11.40 11.60 11.80 5000 31 45 m/z 73.00 2 6.29% 103

m/z-? Abundance 20 .. . ... 1 1_______ _ ______ __________ 134 ■ i '• ■ ■ i • • • • i• » > • i • • » •| * » • • । < » « » । » > i * । * < i * । « < * » । * < * * । । > । । । ri i । । । 30 40 50 60 70 80 90 #6087: 2-Propanol, 1,1’-oxybis- 59 100 110 120 130 140 111r

m/z . ] ■ i । 11.00 11.20 11.40 11.60 11.80 41.05 ।

20.65% । ’

31

NN 5000 45 103

111 > > । ci > 1111 72......... ............................. ..... — • i * • • ■ < •■ ■ • i 1 1'1 I ‘ 1 • ■i • • ■ • 111 1ri ■ ।i । | i r* ‘ ‘ I 1nnB/B/nnBBEnT m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80

29141.D GCMS1126.M Wed Dec 12 16:08:37 2001 Page 4

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