GCMS sample analysis AD29291, Dec 2001

NYC 9/11 Public Portal D. ocument

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1001\29235.D Vial: 8 Acq On : 12 Dec 2001 6:34 am Operator: 209 GALOS Sample : gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 1.05 ug/1 269635 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, -(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 90 2 2-Propanols 1,1’ -oxybis- 134 C6H14O3 000110-98-5 56 3 2-Butanol/ 3,3' -oxybis- 162 C8H18O3 054305-61-2 50 4 1-Propancl ,2- (2-hydroxypropoxy) - 134 C6H14O3 000106-62-7 42 Abundance Scan 696 (11.431 min): 29235.D (-) m/z 59.05 100.00% 59

miz-2 5000

20 h 1139, 30 45

1+ +D 1 1 ■ i • 1 1 1 i ■ 1 ■ • TT i । 40 50 60 70 73

80 86 90 94 103

100 , 110 । 120 । i ... । . 130 140 m/z JU 11.20 11.40 11.60 11.80 45 05 1 1 1 1 ‘

45.90% Abundance ;#9238:2-Propanol, 1-(2-methoxy-1-methylethoxy j- 59 V 5000 TOuuuTTTTT 45 103 11.20 11.40 11.60 11.80 73 31 m/z 103.05 34.37% TT i ■ ■ ■ ■ i ■ -PPI -0 miz-> 20 ' ‘ 30 140 50 60 70 80 90 100 110 120 130 140 Abundance #6087: 2-Propanol, 1,1-oxybis- 59 - 31 11.20 11.40 11.60 11.80 5000 45 m/z 73.00 28.13% 103

m/z-> t...... _ 20 30__ 40__50__ 60__ 70 80 90 100 110 120 130 140 Abundance #12859:2-Butanoi, 3,3‘-oxybis- 1. . • » r jl .1 ’I’ I 59 11.20 11.40 11.60 11.80 m/z 5000 31 45 103

■ I ' — PPP + 1 i 1 — 1pTmm I IT TT । i । । । । । 1 1 1 i ■ ■ • • i • • 1 • l 134 • • • • i 1 ===== --------- m/z~> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.20 11.40 11.60 11.80

29235.D GCMS1126.M Wed Dec 19 12:53:14 2001 Page 3 NYC-WTC_000036241