GCMS analysis results for sample AD29932, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1801\29962.D Vial: 11 Acq On 19 Dec 2001 1:51 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 4.06 ug/1 1185140 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 4 Pentane, 3-methoxy­ 102 C6H140 036839-67-5 9 Abundance 70 Scan 278 (7.596 min): 29962.D (-) m/z 73.00 100.00% . 73

5000 43

103 7.20 7.40 7.60 7.80 8.00 38 I, I 48 5,5 60 67, । l( ■ ■ i > < 87 '■' I1 11 1 I ''' । i‘| ' ' ' ' | •' • i ■ • > । । ‘ ■ i ■ m/z 43.00 28.74% m/z-> 10 20 30 40 50 60 71 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

5000 - 58 7.20 7.40 7.60 7.80 8.00 44 m/z 4 ! . 05 10.46% 15 | 4 .. i ' ■ ■ ■ i i ■ ■ I • 1 ' ' i ' 1 ' ' I ' ‘ 1 1 I ■ ‘ ■ I ’ ' ' ' I ' ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902: 1,3-Dioxolane, 2-methyl- 73 TIT T । , , TrTrr 7.20 7.40 7.60 7.80 8.00 5000 43 m/ z 45.05 10.22% 58 27 87 ' ' I ' ' ' ' I ii. < -FT-j-T-r-r-r-j-r-, , , । . . . . । . 1 ........... m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 1 I ' ' 1 P T 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.54%. 5000-

45

m/z~> 15 TTIpr 10 20 .......... 30 40 —50535960......70 1 80 8890 +-n-j i . .-T-f-r-r-T-r-j-i > i i । . . 100 110 TIuuufuu—rinr , TIT 7 20 7.40 7.60 7.80 8.00

29962.D GCMS1126.M Tue Jan 15 15:27:35 2002 Page 1

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