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GC/MS analysis results for sample AD22580, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22580 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087202–000087225

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087211
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22580.D Vial: 8 Acq On : 28 Sep 2001 7:17 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 6.64 0.45 ug/1 65243 1,4-Dichlorobenzene-d4 11.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 :exanol 102 C6H14O 000623-37-0 74 2 J-Pentanol 88 C5H12O 000584-02-1 42 3-Pentanol, 2-methyl- 102 C6H14O 000565-67-3 38 4 Propanoic acid, 2-hydroxy-2-methyl- 118 C5H10O3 002110-78-3 33 Abundance Scan 174 (6.640 min): 22580.D (-) m/z 59.05 100.00% sb

5000 73 43 .......... 6.20 6.40 6.60 6.80 7.00 . 53 84 ... HI. I " ' ‘ I' " ' I" '' I' " ' I m/z 54.95 76.49% nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63528:3-Hexanol sb

73 5000 I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' 31 6.20 6.40 6.60 6.80 7.00 "mT^ 73.00 45.79% 45 84 ... t I"'' I" "I T T P nZz-> 20 25 30 35 40 . 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62942:3-Penfanol Sb

31 6.20 6.40 6.60 6.80 7.00 5000 m/z 43.05 31.22% 41

87 mfe-> Abundance TTri...lr4lTt 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #63561:3-Pentanol, 2-methyl- 5|9 I" ' ‘ I I •''' I

6.20 Aj 6.40 6.60 6.80 7.00 "mTz 41705 25.70% 5000 73

31 45 4 I........ . 85 102 I " ‘' I' I"'*I T'"'^ p m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.20 6.40 6.60 6.80 7.00

22580.D NP091101.M Wed Oct 03 11:37:40 2001 Page 3 NYC-WTC_000087211

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NYC-WTC_000087211Source: NYC Law Department, mirrored locally

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