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GC/MS analysis results for sample AD22653, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22653 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087303–000087325

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087312
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\l\DATA\SEP2801\22653.D Vial: 12 Acq On ; 28 Sep 2001 11:13 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 6.63 0.45 ug/1 56478 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol / 102 C6H14O 000623-37-0 90 2 3-Pentan^ 88 C5H12O 000584-02-1 45 3 3-Pentaja(ol, 2-methyl- 102 C6H14O 000565-67-3 38 4 2-Propanol, 2-methyl-____________ 74 C4H10O 000075-65-0 36 Abundance / Scan 173 (6.631 min); 22653.D (-) m/z 59.05 100.00% 5b ,1 5000 73

41 6.20 6.40 6.60 6.80 7.00 84 I''' 'I'" ' I I'"' I “mTz 54.95 76.33% n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63531; 3-Hexanol 5(9

5000 73 6.20 6.40 6.60 6.80 7.00 43 m/z 73 .'00 49.75% I'''' I'''' r''' I .................. +4 I" " I I'"' I" " I'''' I nZz-> 20 25 30 35 40 .45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #62943; 3-Pentanol

31 5(9

6.20 6.40 /L, 6.60 6.80 7.00 5000 “m/z 41.05 27.76% 41

■nZz-> -.. Ma... I'll trrTTT-rrrrr 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63561; 3-Pentanol, 2-methyl- 5^ 6.20 6.40 6.60 6.80 7.00 m/z 43.00 22.71% 5000 73

nfe-> I" " I ‘' I 31 45 l"irTrrrl|.l 854 102 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 6.20 ' 6.40 w aeo ' iso ' ' 7.00 ' '

22653.D NP091101.M Fri Oct 05 08:56:46 2001 Page 3

NYC-WTC_000087312

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NYC-WTC_000087312Source: NYC Law Department, mirrored locally

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