Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
NYC-WTC_000068559–000068571Folder label: “508 Scan X 10/16/01 A 11/5/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C;\HPCHEM\1\DATA\NOV0501\LB .D Vial: 2 Acq On 5 Nov 2001 12:14 pm Operator: 209 GALOS Sample : 10/16 lab blk Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title ; 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.33 0.41 ug/1 73597 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolFoinn CAS# Qual
1 3 -Hexano: 100 C6H12O 000589-38-8 59 2 3-Penta: me, 2-methyl- 100 C6H12O 000565-69-5 42 3 2,4-Pe anedione 100 C5H8O2 000123-54-6 35 4 Hexi , 3,3,4-trimethyl- 128 C9H20 016747-31-2 28 Abundance 7 Scan 140 (6.327 min): LB.D (-) m/z 43.05 100.00% 4t3 5|7
71 ft 5000 100
34 I 49 , 85 6.00 6.20 6.40 6.60 'I..... I’.... ............................. .............. |,.... m/z BYTOO 96.48% nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357: 3-Hexanone 43 57 29
EQ 71 ' ' I ' ' ' ' I ' ' ‘ ' I ' ‘ ' I 6.00 6.20 6.40 6.60 100 m/z 71.00 65.47%
+t .............. ”......... I r n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63398:3-Pentanone, 2-methyl- 5|7 43 6.00 6.20 6.40 6.60 5000 m/z 100.05 40.65% 100 71 85 1 ’' •' 1'' " I - ttZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63324:2,4-Pentanedione 43 6.00 6.20 6.40 6.60 “m/z 41700 34.68%
522 85 100
58 72 ' I'''' I'''' I'' I' I' “ ' I " '' I' I'' I' " ' I +rrTyrrrrr 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60
LB.D NP103001.M Fri Nov 09 12:14:12 2001 Page 1
NYC-WTC_000068565
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NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088184
Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.992
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NYC-WTC_000068555
Record of a GCMS scan conducted at the World Trade Center site in mid-November 2001.
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NYC-WTC_000068556
Log sheet recording liquid-liquid extraction parameters and sample processing details for November 2001.
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Laboratory report documenting GCMS analysis of sample AD24487 conducted on November 13, 2001, identifying unknown compounds.
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NYC-WTC_000068585
Laboratory report documenting GCMS analysis of sample AD24488 conducted on November 13, 2001, identifying unknown compounds.
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NYC-WTC_000068598
Laboratory report documenting GCMS analysis of sample AD24489 conducted on November 13, 2001, identifying unknown compounds.
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