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Document / 13 pages

GCMS calibration table for TCLP analysis, Oct 25 2001

Machine-extracted title · confidence 95%

Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.

NYC-WTC_000067739–000067751

Folder label: “GCMS Scan X 10/5/01 An 10/25/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\LB.D Vial: 2 Acq On : 25 Oct 2001 11:58 am Operator: 209 GALOS Sample : lab blk 10/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.36 0.49 ug/1 83931 1,4-Dichlorobenzene-d4 11.74 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanone 100 C6H12O 000589-38-8 86 2 3-Pentanone, 2-methyl- 100 C6H12O 000565-69-5 43 3 2,4-Pientanedione 100 C5H8O2 000123-54-6 38 4 Hexane, 2,4,4-trimethyl- 128 C9H20 016747-30-1 33 Abundance/ Soan 143 (6.359 min): LB.D (-) m/z 43.05 100.00%

5000 4)3 57 71 1 100 '' I ■

85 6.00 6.20 6.40 6.60 6.80 4-T +rr m/z” 57.00 78.53% nfe-> 20^ 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105

Ju, Abundance #63358:3-Hexanone 43 57

5000 71 6.00 6.20 6.40 6.60 6.80 100 m/z” 71.00 59.76%

tv - u Tife-> 20^^35 40 45 50 55 60 ^ 70 75 80 85 90 95 100 105 Abundance #63398:3-Pentanone, 2-methyl- 5|7 43 6.00 6.20 6.40 6.60 6.80 5000 m/z 100.05 33.67% 100

iJsu, 71 •m 1 ■ 1111 ■ ■ ■ .... 11 85 +TTTT p Tife-> 20^ 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63324:2,4-P8ntanedione 43 600 6.20 6,40 6.60 6.80 “m/z 41.05 23.69% 5000 85 100

27 58 72 p+ Al p 6.00 6.20 6.40 6.60 6.^ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105

LB.D NP101901.M Mon Oct 29 09:51:44 2001 Page 1 NYC-WTC_000067745

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NYC-WTC_000067745Source: NYC Law Department, mirrored locally

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