Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
NYC-WTC_000067739–000067751Folder label: “GCMS Scan X 10/5/01 An 10/25/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\0CT2 5 01\LB.D Vial: 2 Acq On 25 Oct 2001 11:58 am Operator: 209 GALOS Sample : lab blk 10/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.46 1.00 ug/1 170307 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 , Tentative ID MW MolForm CAS# Qual 1 2-Hexan e 100 C6H12O 000591-78-6 91 2 Methyl sobutyl Ketone 100 C6H12O 000108-10-1 58 3 Oxira: , 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 56 4 2-Pe:; ene, 2-methoxy-__________ 100 C6H12O 061142-47-0 50 Abundance/ Scan 154 (6.460 min): LB.D (-) m/z 42795 100.00% 40 58 5000
' ' ' ' H ' ' ' I ' ' 71 ® 100 6,20 6.40 6.60 6,80 ll....l.Tnih.iiH.t|n..|u rTT,rrrT»r..|t...| ■p m/z 58705 60.92% TlZZ-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1556:2-Hexanone 43
58 5000 . 14 ■ ■ . I^rrn-I ■ ■ I 6.20> 6,40 6.60 6,80 m/z !57.00 19.26% 27 tp' n|ii..|.lll| ^1^ 85 100 I ‘ ‘ ■ I' 71111111111111 I • “ • 111 ■' I■ I ..... nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63351: Methyl Isobutyl Ketone 40 6.20 6.40 6.60 6.80 5000 m/z 41.05 16.11% 58 27
xTybdV 1 • ‘ • 111 ‘ 11 ■ ‘ >>1 85 100 72 +p^ Tlfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1530: Oxirane, 2-methyl-2-(1-methyl^yl)- 40 6.20 6.40 6.60 6.80 58 m/z 84.95 10778% 5000 71 30 66 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.Z) 6.40 6.60 6.80
LB.D NP101901.M Mon Oct 29 09:51:47 2001 Page 2
NYC-WTC_000067746
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NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067940
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 31, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067555
DEP lab report for GCMS analysis of sample AD23909 conducted on October 23, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088184
Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000067735
Record of a GCMS scan conducted at the World Trade Center site in late October 2001.
Filed in the same folder
NYC-WTC_000067736
Header page from a GCMS scan batch dated October 5, 2001, associated with DEP laboratory operations.
Filed in the same folder
NYC-WTC_000067752
Laboratory report documenting GCMS analysis of sample AD23995 conducted on October 29, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000067767
Laboratory report documenting GCMS analysis of sample AD23996 conducted on October 29, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000067782
Laboratory report documenting GCMS analysis of sample AD23997 conducted on October 29, 2001, noting unknown compounds.
Filed in the same folder