Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
NYC-WTC_000067739–000067751Folder label: “GCMS Scan X 10/5/01 An 10/25/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Confound Report Data File : C:\HPCHEM\1\DATA\OCT2501\LB.D vial: 2 Acq On : 25 Oct 2001 11:58 am Operator: 209 GALOS Sample : lab blk 10/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.60 0.42 ug/1 72230 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanol 102 C6H14O 000623-37-0 83 2 Oxiran^ tetramethyl- 100 C6H12O 005076-20-0 58 3 3 - Pen^^nol 88 C5H12O 000584-02-1 45 4 3-Hydroxy-3-methyl-2-butanone 102 C5H10O2 000115-22-0 38 Abundanro^ Scan 169 (6,598 min): LB.D (-) m/z 59705 100700% 50
5000 73 43
6.y 6,40 6.60 6.80 7.00 i„„|t?^ilili|.,„pV. 85 100 I ■ I I I a f I 1 I I I i I • ■ I I I > 1 ( I I . I I I I I ■-] m/z 55.00 83.58% mZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance
L #63527:3-Hexanol 50
5000 73 31 6.20 6X0 6.60 6.80 7.00 m/^ 73.00 46.86% 45 11* >11' I"! Tnj +u 84 IpTTTpTTTpTrrpnTrjTTTTpT^^ ■nfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1579: Oxirane, tetramethyl- 5b 43 ‘ 1 ‘ ‘ 6.y ' I ' ‘ 6,40 6.60 6.80 7.00 »X)0 m/z 43.00 30.74% 31
'nfe-> 5 Abundance 10 15 20 25 45 w ‘ re' /b '75'^ '^‘‘^'iro #62943:3-Pentanol 6.^ “mTz w 6,40 41.05 6.60 6,80 . 7.00 22.14% 31 5000
41
mfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.20 6,40 6.60 6,80 7.00
LB.D NP101901.M Mon Oct 29 09:51:49 2001 Page 3
NYC-WTC_000067747
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NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067940
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 31, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067555
DEP lab report for GCMS analysis of sample AD23909 conducted on October 23, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088184
Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000067735
Record of a GCMS scan conducted at the World Trade Center site in late October 2001.
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NYC-WTC_000067736
Header page from a GCMS scan batch dated October 5, 2001, associated with DEP laboratory operations.
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NYC-WTC_000067752
Laboratory report documenting GCMS analysis of sample AD23995 conducted on October 29, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000067767
Laboratory report documenting GCMS analysis of sample AD23996 conducted on October 29, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000067782
Laboratory report documenting GCMS analysis of sample AD23997 conducted on October 29, 2001, noting unknown compounds.
Filed in the same folder