Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
NYC-WTC_000067739–000067751Folder label: “GCMS Scan X 10/5/01 An 10/25/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\LB.D Vial: 2 Acq On : 25 Oct 2001 11:58 am Operator: 209 G7VLOS Sample : lab blk 10/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Pentanol, 4-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.71 0.60 ug/1 101906 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanol, -methyl- 102 C6H14O 000108-11-2 83 2 2-Hexanol 102 C6H14O 000626-93-7 83 3 2-Butanol/ 74 C4H1O0 000078-92-2 50 4 2-HexanoX/ (S)- 102 C6H14O 052019-78-0 43 Abundance Scan 181 (6.708 min): LB.D (-) m/z 44795 100.00% 4h3 1 5000
41 69 6.40 6.60 6.80 7.00 m/z 69.10 16.56% TiZz-> 10 15 20:S30 35 40 45 50 55 60 65 70 75 80 85 90 95 ft Abundance #1773:2-Pentanol, 4-methyk 4)5
5000 ‘''i 1^1 n I 14-41 'I 6.40 6.60 6.80 7.00 m/z 43.05 12.86% 27 42 I'''' I'''' I'''' I'' " I ) 8487 <1111<11111<I»111111111<1111111»11»»Ij * 11111111111 TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 «^undance #63584:2-Hexanol 43
6.40 6.60 6.80 7.00 5000 m/z 41.00 11.47% 69
nZz-> Abundance 10 19 ^,31 4:^1 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #62568:2-Butenol . I.. .... JdW__ 6.40 6.60 6.80 7.00 m/z 43.90 10.43% 5000
27^1 59 I" “ I ■ • • ■ I > 1 • • I 72 T-rp-n-rp-r . . . I . . . . I . . . . I . . . . , . . . . I n&-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6 40 6 60 6 60 7 00
LB.D NP101901.M Mon Oct 29 09:51:51 2001 Page 4
NYC-WTC_000067748
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NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067940
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 31, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067555
DEP lab report for GCMS analysis of sample AD23909 conducted on October 23, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088184
Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000067735
Record of a GCMS scan conducted at the World Trade Center site in late October 2001.
Filed in the same folder
NYC-WTC_000067736
Header page from a GCMS scan batch dated October 5, 2001, associated with DEP laboratory operations.
Filed in the same folder
NYC-WTC_000067752
Laboratory report documenting GCMS analysis of sample AD23995 conducted on October 29, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000067767
Laboratory report documenting GCMS analysis of sample AD23996 conducted on October 29, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000067782
Laboratory report documenting GCMS analysis of sample AD23997 conducted on October 29, 2001, noting unknown compounds.
Filed in the same folder