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Document / 13 pages

GCMS calibration table for TCLP analysis, Oct 25 2001

Machine-extracted title · confidence 95%

Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.

NYC-WTC_000067739–000067751

Folder label: “GCMS Scan X 10/5/01 An 10/25/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\LB.D Vial: 2 Acq On : 25 Oct 2001 11:58 am Operator: 209 G7VLOS Sample : lab blk 10/5 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Pentanol, 4-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.71 0.60 ug/1 101906 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanol, -methyl- 102 C6H14O 000108-11-2 83 2 2-Hexanol 102 C6H14O 000626-93-7 83 3 2-Butanol/ 74 C4H1O0 000078-92-2 50 4 2-HexanoX/ (S)- 102 C6H14O 052019-78-0 43 Abundance Scan 181 (6.708 min): LB.D (-) m/z 44795 100.00% 4h3 1 5000

41 69 6.40 6.60 6.80 7.00 m/z 69.10 16.56% TiZz-> 10 15 20:S30 35 40 45 50 55 60 65 70 75 80 85 90 95 ft Abundance #1773:2-Pentanol, 4-methyk 4)5

5000 ‘''i 1^1 n I 14-41 'I 6.40 6.60 6.80 7.00 m/z 43.05 12.86% 27 42 I'''' I'''' I'''' I'' " I ) 8487 <1111<11111<I»111111111<1111111»11»»Ij * 11111111111 TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 «^undance #63584:2-Hexanol 43

6.40 6.60 6.80 7.00 5000 m/z 41.00 11.47% 69

nZz-> Abundance 10 19 ^,31 4:^1 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #62568:2-Butenol . I.. .... JdW__ 6.40 6.60 6.80 7.00 m/z 43.90 10.43% 5000

27^1 59 I" “ I ■ • • ■ I > 1 • • I 72 T-rp-n-rp-r . . . I . . . . I . . . . I . . . . , . . . . I n&-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6 40 6 60 6 60 7 00

LB.D NP101901.M Mon Oct 29 09:51:51 2001 Page 4

NYC-WTC_000067748

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NYC-WTC_000067748Source: NYC Law Department, mirrored locally

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Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.

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