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GC/MS analysis results for sample AD23272, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.

NYC-WTC_000088456–000088484

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088465
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23272.D vial: 22 Acq On : 12 Oct 2001 10:39 pm Operator: 2 09 G7VLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanol, 4-methyl- Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 6.74 0.54 ug/1 50535 1,4-Dichlorobenzene-d4 11.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-PentanoX 4-methyl- 102 C6H14O 000108-11-2 83 2 2-Hexanpl 102 C6H14O 000626-93-7 83 3 2-Hex^ol, (S)- 102 C6H14O 052019-78-0 74 4 2-HeXanol, (R)- 102 C6H14O 026549-24-6 64 Abundance / Scan 185 (6.736 min): 23272.D (-) m/z 44.95 107770% 4b

5000

41 69 ' I ' ' '7 5356 Y 84^ 6.40 "rot 6.80 7.00 I"'' I" " I" " I m/z 69.00 16.79% mZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546: 2-Penlanol, 4-methyl- 4b

I A 5000 6.40 6.60 6.80 7.00 27 69 m/T 41.00 14.73% 19 42 57 I W87 .... I ■ 1111 ■' ■ ■) • • ■ ■ I • ■ ■ 11 ■ I ■' I m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1792; 2-Hexanol 43

6.40 660 6.80 7.00 aS m/z 42795 17721%

69 5558 I 8487 .... . I''' 11'' ‘ ‘ I'''' I''' 11' I'' I tn/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1769; 2-Hexanol, (S)- 4b 6.40 6.60 6.80 7.00 m/z 43.90 10.70%

5000

69 rp-r-n-p- .............. ........ 55 I 8487 I'''' I' ' I''' 11'''' I'''' I'''' i'''' I'''' I' ' I ' ' ' ' I ' ' ' ' I m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

23272.D NP091101.M Mon Oct 15 09:41:54 2001 Page 3

NYC-WTC_000088465

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