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GC/MS analysis results for sample AD23082, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23082 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087875–000087892

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\OCT04 0l\23082.D Vial: 2 Acq On 4 Oct 2001 4:30 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Tetratetracontane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

35.52 0.53 ug/1 66210 Perylene-dl2 37.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetratetracontane 619 C44H90 00.7098-22-8 91. 2 Pentatriacontane 493 C35H72 000630-07-9 91 3 Hexatriacontane 507 C36H74 000630-06-8 91 4 Heneicosane 296 .C21H44 ____ 000629-94-7 91 (Abundance Scan 3320 (35.521 min): 23082.D (-) m/z 57?on” 100.00% 5/

5000 85

183 35.20 35.40 35.60 35.80 281 m/z 71.1,0 76.94% m/z->50 100 150 2.QP J50 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontane 5Z

5000 85 35.20 35.40 35.60 35.80 m/z 43.05 64.22% 1 ...... , , I........ A I ni/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #58743: Pentatriacontane 57

35.20 35.40 35.60 35.80 5000 85 m/z 85.0,5 48.37% A

, // P,141169197225.................

a , . m/2-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74636; Hexatriacontane 5(7 35.20 35.40 35.60 35.80 m/z 55.0^0 23.73% 5000 85

■n" T rn/z--> 50 100 150 200 250 300 350 400 450 500 550 600 35.20 35.40 35.60 35.80

23082.D NP091101.M Tue Oct 09 12:24:26 2001 Page 9

NYC-WTC_000087890

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NYC-WTC_000087890Source: NYC Law Department, mirrored locally

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