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GC/MS analysis results for sample AD23080, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23080 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087817–000087841

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

r Data File C:\HPCHEM\1\DATA\OCT0301\23080 .D Vial: 7 Acq On 3 Oct 2001 6:30 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Hexatriacontane Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

36.39 0.62 ug/1 78822 PerYlene-dl2 37.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Tetratetracontane 619 C44H90 007098-22-8 91^ 3 Pentatriacontane 493 C35H72 000630-07-9 91 2 4 Tetracosane 338 C24H50 000646-31-1 91/ /\bundance Scan 3414 (36.386 min): 23080.D (-) m/z 56.95 100.00% 5Z

5000 85

. 36.00 36.20 36.40 36.60 36.80 . L I J J V/5. ^9^ , 281 I m/z 71.00 75.05% jn/Z">___ _ 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74636: Hexatriacontane 57

5000 85 36.00 36.20 36.40 36.60 36.80 m/z 43.0.0 62.06%

m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontane 57

36.00 36.20 36.40 36.60 36.80 5000 ! -85 m/ z 85.0,5 49.02%

' / 169197225 379407 590618 nri/2-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #58743: Pentatriacontane 36.00 36.20 36.40 36.60 36.80 m/z 41.05 28.27% 5000 85

ni/z-> 50 100 f 150 200 .............. 250300 350 400 450 500 550 600 36.00 36.20 36.40 36.60 36.80

23080.D NP091101.M Tue Oct 09 10:02:28 2001 Page 15

NYC-WTC_000087838

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NYC-WTC_000087838Source: NYC Law Department, mirrored locally

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