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GC/MS analysis results for sample AD22777, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22777 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087953–000087972

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document j-iiurciiy cjedxcn compouna Report

Data File : C:\HPCHEM\1\DATA\OCT0401\22777.D Vial: 8 Acq On : 4 Oct 2001 10:23 pm Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Tetracosane Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 33.71 0.81 ug/1 131128 Chrysene-dl2 33.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 9a 2 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 90^ 3 Pentadecane, 8-hexyl- 296 C21H44 013475-75-7 90 / 4 Nonacosane 408 C29H60 000630-03-5 90 Abundance Scan 3123 (33.714 min): 22777.D (-) m/z 57.00 100.00%

43 57 71 (I 85 5000

99 33.40 33.60 33.80 34.00 227 '' I ■ " I'' " 111111" " I " " I " " I'' " I'' m/z 71.00 71.10% nfe-> Abundance 40 60

43 5 7 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73543: Tetracosane (1 71

5000 85 .. .. 33.40 33.60 33.80 34.00 Wz 43705 67.30% ■ I. .M. ll. 155169183197 294 338 I'''' I"''' I''"' I'''' 11' ' 11 r 1 • 11 ■ ■ i’ 11 I'''' I'''' r ''' I'''' I i''' ‘I' T»/z-> . 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #51002: Heneicosane, ll-(l-ethylpropyl)- 43 57 -rV-T 71 33,40 33,60 33,80 34.00 5000 m/z 85.05 51.94% 85 I

183197211225 295 338 I' • I “ 111 I I. II I . I I I I I I ry^TTTiyri-riyi-rTTYrTT-rp-rrr-^^ n/Z“> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42199: Pentadecane, 8-hexyl- 43 517 33.40 33.60 33.80 34.00 in/z 41.05 26.06% 71 5000 85

y113127141 p-m-p-rTTp-r ....... .............................. 266 ,2^.................... T Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 33.40 33.60 33.80 34.00

22777.D NP091101.M Fri Oct 05 12:49:21 2001 Page 8

NYC-WTC_000087967

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NYC-WTC_000087967Source: NYC Law Department, mirrored locally

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