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GC/MS analysis results for sample AD22777, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22777 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087953–000087972

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document ijxurary bearcn compound Report ,Data File : C:\HPCHEM\1\DATA\OCT0401\22777;D Vial: 8 Acq On : 4 Oct 2001 10:23 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Hexatriacontane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 34.63 0.55 ug/1 88938 Chrysene-dl2 33.15 Hit# Of 5 Tentative ID MW MolForm CAS# Qual Hexatriacontane 507 C36H74 000630-06-8 90 2 Heptadecane 240 C17H36 000629-78-7 87 3 Tetradecane 198 C14H30 000629-59-4 87 4 Octacosane 394 C28H58 000630-02-4 86 ^Abundance Scan 3223 (34.632 min): 22777.D (-) m/z SYTOO 100.00% T 71 43 5000 85

T r?".. I . I I Ynf . I . r I ITT 99

■nfe-> Abundance 40 XL 60 80 100 120 140 160 )

#74636: Hexatriacontane ' I I I ■ '180 197 I ' I 200 220 240 260 281 280 m/z 34.40 34.60 34.80 35.00 71.00 71797%

43 57

71 5000 85 34.40 34.60 34.80 35.00 m/z 43.00 61.09% 97

’n/z-> ..... i.. 40 60 J X .'*1^?.?^ 80 100 120 140 160 180 200 220 240 260 280 Abundance #71193: Heptadecane 57

71 34.40 34.60 34.80 35.00 5000 "m/z 85.05 47752% 85

99 440

-n/2-> ' ' I ' ' 40 60 ,1 80I, 100 X, ! 120 140 160 180 ..200........ 220 240 260 280 Abundance 57 71 #69662: Tetradecane 1 34.40 34.60 34.80 35.00 m/z 54.95 24745% 85 5000

113 127 141154 ' I ' ' ' I I' ' I ' II ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 34.40 34.60 34.80 35.00

22777.D NP091101.M Fri Oct 05 12:49:23 2001 Page 9

NYC-WTC_000087968

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NYC-WTC_000087968Source: NYC Law Department, mirrored locally

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